保護柱的填料裝填方式也是選擇保護柱時要考慮的重要因素。目前有兩種填料方式:
(1)薄bo膜mo裝zhuang填tian法fa的de保bao護hu柱zhu,使shi用yong過guo程cheng很hen簡jian單dan方fang便bian,而er且qie可ke以yi在zai實shi驗yan室shi中zhong進jin行xing幹gan裝zhuang。但dan是shi,其qi最zui大da的de缺que點dian是shi不bu經jing濟ji,特te別bie是shi針zhen對dui中zhong國guo的de具ju體ti情qing況kuang,一yi次ci性xing使shi用yong相xiang對dui費fei用yong較jiao高gao。另ling外wai,薄bo膜mo裝zhuang填tian法fa的de保bao護hu柱zhu所suo裝zhuang填tian的de色se譜pu填tian料liao有you限xian,隻zhi能neng提ti供gong很hen有you限xian的de保bao護hu作zuo用yong;不過也因為所裝填的色譜填料較少,保護柱的長度也較短,所以對分析樣品的保留時間的影響也很小。
(2)還有一種保護柱結構其實質是縮短了的色譜分析柱,設計方式上有直連式、手shou緊jin式shi或huo整zheng體ti式shi。整zheng體ti式shi設she計ji是shi由you色se譜pu柱zhu的de生sheng產chan廠chang商shang直zhi接jie安an裝zhuang在zai色se譜pu分fen析xi柱zhu上shang的de,必bi須xu與yu色se譜pu分fen析xi柱zhu一yi同tong訂ding貨huo,可ke以yi非fei常chang方fang便bian地di使shi用yong,但dan不bu能neng夠gou被bei修xiu改gai。直zhi連lian式shi結jie構gou設she計ji可ke在zai任ren何he時shi候hou由you色se譜pu工gong作zuo者zhe來lai安an裝zhuang連lian接jie,可ke以yi與yu任ren何he品pin牌pai的de色se譜pu分fen析xi柱zhu連lian接jie使shi用yong,而er且qie還hai可ke以yi根gen據ju樣yang品pin的de相xiang關guan情qing況kuang選xuan擇ze不bu同tong的de保bao護hu柱zhu長chang度du。手shou緊jin式shi保bao護hu柱zhu從cong結jie構gou上shang講jiang是shi與yu直zhi連lian式shi保bao護hu柱zhu一yi樣yang,隻zhi是shi在zai連lian接jie時shi不bu需xu要yao借jie助zhu扳ban手shou等deng工gong具ju,直zhi接jie用yong手shou上shang緊jin即ji可ke。另ling外wai從cong保bao護hu柱zhu結jie構gou的de角jiao度du看kan,保bao護hu柱zhu的de結jie構gou又you分fen為wei是shi否fou可ke以yi更geng換huan保bao護hu柱zhu柱zhu芯xin。現xian在zai大da多duo數shu的de保bao護hu柱zhu均jun可ke以yi更geng換huan保bao護hu柱zhu柱zhu芯xin,可ke以yi降jiang低di保bao護hu柱zhu的de使shi用yong成cheng本ben。大da多duo數shu人ren是shi根gen據ju色se譜pu分fen析xi柱zhu的de填tian料liao選xuan擇ze保bao護hu柱zhu的de填tian料liao,正zheng常chang情qing況kuang下xia可ke以yi選xuan擇ze與yu分fen析xi色se譜pu柱zhu一yi樣yang的de色se譜pu填tian料liao。但dan是shi,根gen據ju實shi際ji的de分fen析xi工gong作zuo,也ye可ke不bu必bi與yu分fen析xi色se譜pu柱zhu的de填tian料liao完wan全quan相xiang匹pi配pei。
總之,對於選擇保護柱的原則是:在滿足分析分離要求的前提條件下,盡可能地選擇較短的保護柱結構,盡可能選擇對分離樣品小一些保留性的填料。
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