(1)電子天平
dianzitianpingshiwomendehuaxueshiyanzhongbibeidechenglianggongju,xueshengyejibennengzhangwoqishiyongfangfa,danshiyandexijiehedasaoweihuzuodehenbudaowei,shiyanhouchengpanxiacanliuyouyixiewuzhi,chengpanshangliuyouwuzi。shitianpingdelingminduhezhunqueduxiajiang,shiyongshoumingyesuoduan。dianzitianpingshiyongqianxuxianyure10分fen鍾zhong,但dan部bu分fen學xue生sheng開kai機ji後hou直zhi接jie稱cheng量liang。稱cheng量liang物wu的de溫wen度du必bi須xu與yu天tian平ping溫wen度du相xiang同tong,不bu能neng把ba過guo熱re或huo過guo冷leng的de物wu體ti放fang在zai天tian平ping秤cheng盤pan上shang。一yi些xie具ju有you揮hui發fa性xing的de腐fu蝕shi性xing的de試shi劑ji應ying放fang在zai密mi閉bi容rong器qi中zhong稱cheng量liang,稱cheng量liang物wu體ti時shi要yao切qie記ji關guan閉bi天tian平ping的de側ce門men,稱cheng量liang完wan畢bi後hou及ji時shi打da掃sao稱cheng量liang盤pan上shang下xia及ji各ge個ge角jiao落luo等deng。在zai空kong氣qi潮chao濕shi,物wu質zhi已yi結jie成cheng垢gou塊kuai時shi,應ying采cai用yong機ji械xie除chu鏽xiu方fang法fa,即ji先xian用yong鏟chan、剔、刮等方式將零部件上的鏽蝕層塊除去,再用砂紙砂磨、打光,最後塗上保護層。實驗完畢,關閉側門,蓋上天平布,置於避光幹燥處保存。
(2)電熱恒溫幹燥箱
電熱恒溫幹燥箱是化學實驗中用於對物品進行烘焙、幹燥的常規儀器。幹燥箱的工作電壓為220V,溫度為100-110度du,不bu宜yi過guo高gao。可ke燃ran性xing和he揮hui發fa性xing的de化hua學xue物wu品pin切qie勿wu放fang入ru箱xiang內nei,箱xiang內nei載zai物wu應ying擺bai放fang應ying在zai隔ge板ban的de較jiao中zhong心xin部bu位wei,同tong時shi不bu影ying響xiang空kong氣qi流liu通tong以yi保bao證zheng箱xiang內nei溫wen度du均jun勻yun。幹gan燥zao箱xiang使shi用yong過guo程cheng中zhong,學xue生sheng不bu能neng用yong濕shi手shou觸chu摸mo箱xiang體ti和he開kai關guan。幹gan燥zao箱xiang正zheng常chang運yun行xing時shi如ru在zai使shi用yong過guo程cheng中zhong出chu現xian異yi常chang、氣味、煙yan霧wu等deng情qing況kuang,應ying立li即ji關guan閉bi電dian源yuan,請qing專zhuan業ye人ren員yuan查zha看kan修xiu理li。箱xiang壁bi內nei膽dan和he設she備bei表biao麵mian要yao經jing常chang擦ca拭shi,以yi保bao持chi清qing潔jie,增zeng加jia玻bo璃li的de透tou明ming度du。幹gan燥zao箱xiang若ruo長chang期qi不bu用yong,應ying拔ba掉diao電dian源yuan線xian以yi防fang止zhi設she備bei損sun傷shang人ren,並bing應ying定ding期qi按an使shi用yong條tiao件jian運yun行xing2-3天,以驅除電器部分的潮氣,避免損壞有關器件。
(3)恒溫水浴鍋
恒溫水浴鍋主要用於實驗室中蒸餾,幹燥,濃縮化學藥品,也可用於恒溫加熱和其它溫度試驗,是化學實驗室、分析室、jiaoyukeyandebibeigongju。zaishiyongzhongxueshengyinggaizhidaotadeshiyongfangfajizhuyishixiang,yibianshiyannenggoushunlijinxing。jiashuizhiqianqiewujietongdianyuan,zuihaojiaruzhengliushui,yimianchanshengshuigou,jiashuibuyaotaiduo,yimianfeitengshishuiliangyichuguowai;鍋內水量也不可低於二分之一,不能使加熱管露出水麵;切(qie)勿(wu)無(wu)水(shui)或(huo)水(shui)位(wei)低(di)於(yu)隔(ge)板(ban)加(jia)熱(re),否(fou)則(ze)會(hui)損(sun)壞(huai)加(jia)熱(re)管(guan)。注(zhu)水(shui)時(shi)不(bu)能(neng)將(jiang)水(shui)流(liu)入(ru)控(kong)製(zhi)箱(xiang)內(nei),以(yi)防(fang)發(fa)生(sheng)觸(chu)電(dian)。如(ru)恒(heng)溫(wen)控(kong)製(zhi)失(shi)靈(ling),可(ke)將(jiang)控(kong)製(zhi)器(qi)上(shang)的(de)銀(yin)接(jie)點(dian)用(yong)細(xi)砂(sha)布(bu)擦(ca)亮(liang)。使(shi)用(yong)完(wan)畢(bi)後(hou),取(qu)出(chu)恒(heng)溫(wen)物(wu),關(guan)閉(bi)電(dian)源(yuan),排(pai)除(chu)箱(xiang)體(ti)內(nei)的(de)水(shui),做(zuo)好(hao)儀(yi)器(qi)使(shi)用(yong)記(ji)錄(lu)。
(1)燒杯
燒杯因其口徑上下一致,是取用液體、配製溶液、zuojiandanhuaxuefanyingzuichangyongdefanyingrongqi。danshaobeibunengdaitiliangtongliangquyeti。shaobeijiareshiyaodianshangshimianwang。bunengyonghuoyanzhijiejiareshaobei。yinweishaobeidimianda,yonghuoyanzhijiejiare,zhikeshaodaojubu,shibolishourebuyuneryinqizhalie。yongshaobeijiareyetishi,yetideliangyibuchaoguoshaobeirongjide1/3為(wei)宜(yi),以(yi)防(fang)沸(fei)騰(teng)時(shi)液(ye)體(ti)外(wai)溢(yi)。加(jia)熱(re)時(shi),燒(shao)杯(bei)外(wai)壁(bi)須(xu)擦(ca)幹(gan)。加(jia)熱(re)腐(fu)蝕(shi)性(xing)藥(yao)品(pin)時(shi),可(ke)將(jiang)一(yi)表(biao)麵(mian)皿(min)蓋(gai)在(zai)燒(shao)杯(bei)口(kou)上(shang),以(yi)免(mian)液(ye)體(ti)濺(jian)出(chu)。不(bu)可(ke)用(yong)燒(shao)杯(bei)長(chang)期(qi)盛(sheng)放(fang)化(hua)學(xue)藥(yao)品(pin),以(yi)免(mian)落(luo)入(ru)塵(chen)土(tu)和(he)使(shi)溶(rong)液(ye)中(zhong)的(de)水(shui)分(fen)蒸(zheng)發(fa)。溶(rong)解(jie)或(huo)稀(xi)釋(shi)過(guo)程(cheng)中(zhong),用(yong)玻(bo)璃(li)棒(bang)攪(jiao)拌(ban)時(shi),不(bu)要(yao)觸(chu)及(ji)杯(bei)底(di)或(huo)杯(bei)壁(bi)。
(2)試管
實驗室用來盛放少量藥品,加熱情況下少量試劑反應的容器。裝溶液時不超過試管容量的1/2,加熱時不超過試管的1/3。取塊狀固體放入試管要用鑷子,不能使固體直接墜入試管中,防止試管底破裂。加熱時使用試管夾,試管夾應夾在距管口1/3處。試管口不能對著人。試管不可以直接加熱,要先預熱,加熱盛有固體的試管時,管口略向下,加熱液體時傾斜約45°。加jia熱re時shi要yao保bao持chi試shi管guan外wai壁bi沒mei有you水shui珠zhu,防fang止zhi受shou熱re不bu均jun勻yun而er爆bao裂lie。加jia熱re後hou不bu能neng驟zhou冷leng,防fang止zhi試shi管guan破po裂lie。加jia熱re後hou不bu能neng在zai試shi管guan未wei冷leng卻que至zhi室shi溫wen時shi就jiu洗xi滌di試shi管guan。加jia熱re時shi應ying用yong外wai焰yan。
(3)容量瓶
容(rong)量(liang)瓶(ping)主(zhu)要(yao)用(yong)於(yu)準(zhun)確(que)地(di)配(pei)製(zhi)一(yi)定(ding)摩(mo)爾(er)濃(nong)度(du)的(de)溶(rong)液(ye),它(ta)是(shi)一(yi)種(zhong)細(xi)長(chang)頸(jing),梨(li)形(xing)的(de)平(ping)底(di)玻(bo)璃(li)瓶(ping),帶(dai)有(you)磨(mo)口(kou)玻(bo)璃(li)塞(sai),瓶(ping)頸(jing)上(shang)刻(ke)有(you)標(biao)線(xian),當(dang)瓶(ping)內(nei)液(ye)體(ti)在(zai)所(suo)指(zhi)定(ding)溫(wen)度(du)下(xia)達(da)到(dao)標(biao)線(xian)處(chu)時(shi),其(qi)體(ti)積(ji)即(ji)為(wei)瓶(ping)上(shang)所(suo)注(zhu)明(ming)的(de)容(rong)積(ji)數(shu)。容(rong)量(liang)瓶(ping)不(bu)能(neng)配(pei)製(zhi)其(qi)容(rong)積(ji)以(yi)下(xia)體(ti)積(ji)的(de)溶(rong)液(ye),即(ji)其(qi)容(rong)積(ji)為(wei)多(duo)大(da),就(jiu)隻(zhi)能(neng)配(pei)製(zhi)多(duo)大(da)體(ti)積(ji)的(de)溶(rong)液(ye)。容(rong)量(liang)瓶(ping)使(shi)用(yong)前(qian)應(ying)先(xian)檢(jian)查(zha)是(shi)否(fou)漏(lou)水(shui),依(yi)次(ci)用(yong)自(zi)來(lai)水(shui),蒸(zheng)餾(liu)水(shui)洗(xi)好(hao)備(bei)用(yong)。將(jiang)溶(rong)質(zhi)在(zai)燒(shao)杯(bei)中(zhong)溶(rong)解(jie)後(hou)轉(zhuan)移(yi)到(dao)容(rong)量(liang)瓶(ping)裏(li),不(bu)能(neng)在(zai)容(rong)量(liang)瓶(ping)裏(li)進(jin)行(xing)溶(rong)質(zhi)的(de)溶(rong)解(jie),控(kong)製(zhi)溶(rong)解(jie)溶(rong)質(zhi)的(de)蒸(zheng)餾(liu)水(shui)量(liang)。轉(zhuan)移(yi)時(shi)必(bi)須(xu)用(yong)玻(bo)璃(li)棒(bang)引(yin)流(liu)。容(rong)量(liang)瓶(ping)不(bu)能(neng)進(jin)行(xing)加(jia)熱(re),如(ru)果(guo)溶(rong)質(zhi)在(zai)溶(rong)解(jie)過(guo)程(cheng)中(zhong)放(fang)熱(re),要(yao)待(dai)溶(rong)液(ye)冷(leng)卻(que)後(hou)再(zai)進(jin)行(xing)轉(zhuan)移(yi),因(yin)為(wei)溫(wen)度(du)升(sheng)高(gao)瓶(ping)體(ti)將(jiang)膨(peng)脹(zhang),所(suo)量(liang)體(ti)積(ji)就(jiu)會(hui)不(bu)準(zhun)確(que)。用(yong)於(yu)洗(xi)滌(di)燒(shao)杯(bei)的(de)溶(rong)劑(ji)總(zong)量(liang)不(bu)能(neng)超(chao)過(guo)容(rong)量(liang)瓶(ping)的(de)標(biao)線(xian),一(yi)旦(dan)超(chao)過(guo),必(bi)須(xu)重(zhong)新(xin)進(jin)行(xing)配(pei)置(zhi)。配(pei)製(zhi)好(hao)的(de)溶(rong)液(ye)轉(zhuan)移(yi)至(zhi)試(shi)劑(ji)瓶(ping)中(zhong)保(bao)存(cun),容(rong)量(liang)瓶(ping)隻(zhi)能(neng)配(pei)製(zhi)溶(rong)液(ye),不(bu)能(neng)儲(chu)存(cun)溶(rong)液(ye),因(yin)為(wei)溶(rong)液(ye)可(ke)能(neng)會(hui)對(dui)瓶(ping)體(ti)進(jin)行(xing)腐(fu)蝕(shi),從(cong)而(er)使(shi)容(rong)量(liang)瓶(ping)的(de)精(jing)度(du)受(shou)到(dao)影(ying)響(xiang)。容(rong)量(liang)瓶(ping)使(shi)用(yong)完(wan)畢(bi)應(ying)及(ji)時(shi)用(yong)水(shui)衝(chong)洗(xi)幹(gan)淨(jing),塞(sai)上(shang)瓶(ping)塞(sai),並(bing)在(zai)塞(sai)子(zi)與(yu)瓶(ping)口(kou)之(zhi)間(jian)夾(jia)一(yi)條(tiao)紙(zhi)條(tiao),防(fang)止(zhi)瓶(ping)塞(sai)與(yu)瓶(ping)口(kou)粘(zhan)連(lian)。最(zui)後(hou)記(ji)錄(lu)溶(rong)液(ye)體(ti)積(ji)的(de)時(shi)候(hou)一(yi)般(ban)保(bao)留(liu)4位有效數字(XXX.0mL)。
(4)滴定管
滴定管是可放出不固定量液體的量出式玻璃儀器,主要用於滴定分析中對滴定劑體積的測量。能精確到0.01mL。帶玻璃活塞的滴定管為酸式滴定管,帶有內裝玻璃球的橡皮管的滴定管為堿式滴定管。酸式、堿式滴定管不能混用,酸式滴定管裝酸性物質和大多數中性物質(尤其是強氧化劑),堿式滴定管裝堿性物質(包括堿和堿性鹽),滴定管使用前先檢查是否漏液,如果漏水,應重新將活塞塗凡士林油。裝液前要用洗液、水shui依yi次ci衝chong洗xi幹gan淨jing,並bing要yao用yong待dai裝zhuang的de溶rong液ye潤run洗xi滴di定ding管guan。將jiang操cao作zuo溶rong液ye倒dao入ru,直zhi到dao充chong滿man至zhi零ling刻ke度du線xian以yi上shang為wei止zhi。注zhu意yi檢jian查zha滴di定ding管guan的de出chu口kou管guan是shi否fou充chong滿man溶rong液ye,如ru有you氣qi泡pao進jin行xing排pai氣qi泡pao操cao作zuo。調tiao整zheng液ye麵mian時shi,使shi液ye麵mian保bao持chi在zai“0”或“0”以yi下xia的de某mou一yi定ding刻ke度du。進jin行xing滴di定ding時shi,應ying將jiang滴di定ding管guan垂chui直zhi地di夾jia在zai滴di定ding管guan夾jia上shang,如ru使shi用yong的de是shi堿jian式shi滴di定ding管guan,拇mu指zhi與yu食shi指zhi在zai玻bo璃li珠zhu所suo在zai部bu位wei一yi旁pang捏nie乳ru膠jiao管guan,不bu要yao捏nie玻bo璃li珠zhu,也ye不bu能neng使shi其qi上shang下xia移yi動dong。滴di定ding時shi應ying逐zhu滴di連lian續xu滴di加jia,接jie近jin終zhong點dian時shi,隻zhi加jia一yi滴di或huo半ban滴di,至zhi溶rong液ye出chu現xian明ming顯xian的de顏yan色se變bian化hua。讀du數shu時shi,手shou拿na滴di定ding管guan上shang部bu無wu刻ke度du處chu,使shi滴di定ding管guan保bao持chi垂chui直zhi,視shi線xian平ping視shi溶rong液ye的de凹ao液ye麵mian,讀du到dao小xiao數shu點dian後hou第di二er位wei,即ji估gu計ji到dao0.01mL。滴定結束後,管內剩餘的溶液應棄去,不得將其倒回原瓶,隨即清洗滴定管,並倒掛於鐵架台上。
實驗室常用的玻璃儀器如燒杯、試管、滴定管、移液管、容量瓶等。儀器在使用中會沾上油汙,水垢,鏽跡等,使用後不及時完全的清洗,會造成結果誤差,甚至會對儀器的壽命、性能會產生極其不良的影響。因此,化學實驗使用的玻璃儀器必須洗滌幹淨。下麵介紹一些玻璃儀器的洗滌方法。
附fu有you易yi去qu除chu物wu質zhi的de簡jian單dan儀yi器qi,如ru試shi管guan。燒shao杯bei等deng,先xian用yong自zi來lai水shui衝chong洗xi,再zai用yong試shi管guan刷shua蘸zhan取qu合he成cheng洗xi滌di劑ji刷shua洗xi,最zui後hou自zi來lai水shui衝chong洗xi。當dang倒dao置zhi儀yi器qi,器qi壁bi形xing成cheng一yi層ceng均jun勻yun的de水shui膜mo,不bu成cheng股gu流liu下xia時shi,即ji已yi洗xi淨jing。
有油汙的玻璃器皿,先用堿性酒精洗滌液洗滌,然後用洗衣粉水或肥皂水洗滌,再用自來水衝洗幹淨。
有鏽跡,水垢的器皿,用(1+3)鹽酸洗液浸泡,再用再來水衝洗幹淨。
有凡士林油汙的器皿,先將凡士林擦去,再用洗衣粉水或肥皂水洗燒煮,取出後用自來水衝洗幹淨。
一些構造比較精細、複雜的玻璃儀器,如容量瓶、移液管等,無法用毛刷刷洗,可以用洗滌液浸泡一定時間,再進行清洗。
洗淨的玻璃儀器不要再用手、布或紙擦拭,以免重新汙染。
實驗室常用的光學儀器如分光光度計、折光計的棱鏡、玻片等,都是一些精密光學儀器,在使用和保養中,必須細心謹慎,嚴格按說明使用,不得任意鬆動儀器各連接部分,不得跌落、碰peng撞zhuang儀yi器qi,以yi防fang止zhi光guang學xue零ling件jian損sun傷shang及ji影ying響xiang精jing度du。被bei測ce試shi樣yang中zhong不bu應ying有you硬ying性xing雜za質zhi,當dang測ce試shi固gu體ti試shi樣yang時shi,應ying防fang止zhi把ba折zhe射she棱leng鏡jing表biao麵mian拉la毛mao或huo產chan生sheng壓ya痕hen。使shi用yong完wan畢bi後hou,嚴yan禁jin直zhi接jie放fang入ru水shui中zhong清qing洗xi,避bi免mian光guang學xue係xi統tong管guan路lu進jin水shui。打da開kai棱leng鏡jing,用yong擦ca鏡jing紙zhi輕qing輕qing擦ca幹gan,不bu論lun在zai任ren何he情qing況kuang下xia,不bu允yun許xu用yong擦ca鏡jing紙zhi以yi外wai的de任ren何he東dong西xi接jie觸chu到dao棱leng鏡jing,以yi免mian損sun壞huai它ta的de光guang學xue平ping麵mian。儀yi器qi應ying存cun放fang於yu幹gan燥zao、無灰塵、無油汙和無有害、易燃、易爆等氣體的地方,以免光學零件腐蝕或生黴。
光學儀器在使用中容易沾上油汙、水濕性汙物、指紋等,影響成像及透光率。清洗折光計的棱鏡、平麵鏡、xianweijingdejingtou,xianyongzhengliushuijinxingqingxi,jingmianruoyouwuzi,keyiyongyichunheyimidehunheyeqingxi。qingxishiyongzhuanmendecajingzhihuomianqiuzhanyoushaoliangqingxiji,shunzheyigefangxiangcashi,congjingtouzhongxinxiangwaizuoyuanyundong,qiejibazheleijingtoujinpaozaiqingxijizhongqingxi。qingxijingtoubudeyonglishica,fouzehuihuashangzengtoumo,sunhuaijingtou。qingxiwanbihouyongcajingzhicagan,biguangbaocun。
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