1.分析天平在使用前沒有經過校準
一(yi)台(tai)分(fen)析(xi)天(tian)平(ping)在(zai)使(shi)用(yong)之(zhi)前(qian),首(shou)先(xian)要(yao)確(que)認(ren)它(ta)的(de)正(zheng)確(que)性(xing)是(shi)否(fou)合(he)格(ge),否(fou)則(ze)該(gai)天(tian)平(ping)所(suo)稱(cheng)量(liang)的(de)正(zheng)確(que)性(xing)得(de)不(bu)到(dao)保(bao)證(zheng)。分(fen)析(xi)天(tian)平(ping)從(cong)首(shou)次(ci)使(shi)用(yong)起(qi),應(ying)對(dui)其(qi)定(ding)期(qi)校(xiao)準(zhun)。連(lian)續(xu)使(shi)用(yong)的(de)天(tian)平(ping),大(da)約(yue)每(mei)星(xing)期(qi)校(xiao)準(zhun)一(yi)次(ci)。校(xiao)準(zhun)時(shi)應(ying)按(an)規(gui)定(ding)程(cheng)序(xu)進(jin)行(xing),必(bi)須(xu)使(shi)用(yong)標(biao)準(zhun)砝(fa)碼(ma)進(jin)行(xing)校(xiao)準(zhun),否(fou)則(ze)將(jiang)起(qi)不(bu)到(dao)校(xiao)準(zhun)的(de)作(zuo)用(yong)。
2.分析天平安裝不正確
在安裝分析天平時首先要選擇選防塵、防潮、防震、防風、防曬、hengwendefangjianzuoweitianpingshi。qici,tianpingyinganfangzailaogukekaodegongzuotaishang,bingxuanzeshidangdeweizhianfang。tianpinganzhuangqian,yinganzhuangxiangqingdanjinxingqingdian,kangebujianshifouqiquan、完wan好hao,並bing對dui天tian平ping的de所suo有you部bu件jian進jin行xing仔zai細xi清qing潔jie。安an裝zhuang時shi,應ying參can照zhao天tian平ping的de說shuo明ming書shu正zheng確que裝zhuang配pei天tian平ping。安an裝zhuang完wan畢bi後hou應ying再zai次ci檢jian查zha各ge部bu分fen安an裝zhuang是shi否fou正zheng常chang,然ran後hou檢jian查zha電dian源yuan電dian壓ya是shi否fou符fu合he天tian平ping的de要yao求qiu,打da開kai天tian平ping檢jian查zha是shi否fou正zheng常chang。
3.環境及樣品的物理因素影響
在使用分析天平進行稱量的過程中,環境和物理因素會對稱量結果產生幹擾,如溫度、樣品揮發、吸濕、磁力、靜電等的幹擾。
(1)溫度的變化對分析天平的影響
如(ru)果(guo)在(zai)稱(cheng)量(liang)過(guo)程(cheng)中(zhong)發(fa)現(xian)顯(xian)示(shi)值(zhi)單(dan)方(fang)向(xiang)漂(piao)移(yi),就(jiu)有(you)可(ke)能(neng)是(shi)溫(wen)度(du)變(bian)化(hua)所(suo)產(chan)生(sheng)的(de)影(ying)響(xiang)。若(ruo)樣(yang)品(pin)與(yu)周(zhou)圍(wei)環(huan)境(jing)之(zhi)間(jian)的(de)溫(wen)度(du)存(cun)在(zai)差(cha)異(yi),則(ze)這(zhe)個(ge)溫(wen)度(du)差(cha)異(yi)就(jiu)會(hui)導(dao)致(zhi)沿(yan)稱(cheng)重(zhong)容(rong)器(qi)流(liu)動(dong)的(de)氣(qi)流(liu)。空(kong)氣(qi)沿(yan)著(zhe)容(rong)器(qi)外(wai)側(ce)流(liu)動(dong)產(chan)生(sheng)一(yi)個(ge)向(xiang)上(shang)的(de)作(zuo)用(yong)力(li),這(zhe)個(ge)力(li)就(jiu)導(dao)致(zhi)稱(cheng)重(zhong)結(jie)果(guo)產(chan)生(sheng)錯(cuo)誤(wu):樣(yang)品(pin)在(zai)動(dong)態(tai)浮(fu)力(li)作(zuo)用(yong)下(xia),稱(cheng)得(de)的(de)重(zhong)量(liang)比(bi)實(shi)際(ji)要(yao)輕(qing)。這(zhe)個(ge)作(zuo)用(yong)直(zhi)到(dao)溫(wen)度(du)平(ping)衡(heng)形(xing)成(cheng)以(yi)後(hou)才(cai)會(hui)終(zhong)止(zhi)。當(dang)把(ba)樣(yang)品(pin)從(cong)幹(gan)燥(zao)爐(lu)或(huo)冰(bing)箱(xiang)中(zhong)取(qu)出(chu)以(yi)後(hou),要(yao)等(deng)到(dao)樣(yang)品(pin)溫(wen)度(du)與(yu)實(shi)驗(yan)室(shi)或(huo)稱(cheng)量(liang)室(shi)溫(wen)度(du)一(yi)致(zhi)時(shi)才(cai)可(ke)以(yi)稱(cheng)量(liang)。樣(yang)品(pin)要(yao)放(fang)在(zai)表(biao)麵(mian)積(ji)盡(jin)可(ke)能(neng)小(xiao)的(de)去(qu)皮(pi)容(rong)器(qi)中(zhong),取(qu)放(fang)稱(cheng)量(liang)容(rong)器(qi)要(yao)使(shi)用(yong)鑷(nie)子(zi)夾(jia)取(qu),而(er)不(bu)能(neng)將(jiang)手(shou)放(fang)入(ru)稱(cheng)量(liang)室(shi)中(zhong)。
(2)樣品吸濕或揮發對稱量結果的影響
如果在稱量的過程中顯示值單方向持續漂移,則可能測量的是揮發性或吸濕性樣品。若樣品吸濕性較強,則重量會增大;若(ruo)被(bei)測(ce)量(liang)樣(yang)品(pin)屬(shu)易(yi)揮(hui)發(fa)物(wu)質(zhi),則(ze)重(zhong)量(liang)會(hui)減(jian)小(xiao)。對(dui)於(yu)吸(xi)濕(shi)性(xing)或(huo)揮(hui)發(fa)性(xing)樣(yang)品(pin)可(ke)使(shi)用(yong)細(xi)頸(jing)容(rong)器(qi),給(gei)容(rong)器(qi)加(jia)蓋(gai)或(huo)上(shang)塞(sai),使(shi)用(yong)清(qing)潔(jie)幹(gan)燥(zao)的(de)稱(cheng)重(zhong)容(rong)器(qi)並(bing)保(bao)持(chi)稱(cheng)盤(pan)上(shang)不(bu)粘(zhan)有(you)灰(hui)塵(chen)、汙染物及水滴。
(3)樣品或容器帶靜電對稱量結果的影響
如(ru)果(guo)每(mei)次(ci)稱(cheng)量(liang)都(dou)顯(xian)示(shi)不(bu)同(tong)的(de)稱(cheng)量(liang)結(jie)果(guo)或(huo)顯(xian)示(shi)值(zhi)不(bu)穩(wen)定(ding),或(huo)稱(cheng)量(liang)結(jie)果(guo)的(de)重(zhong)複(fu)性(xing)差(cha),則(ze)可(ke)考(kao)慮(lv)是(shi)稱(cheng)量(liang)容(rong)器(qi)或(huo)者(zhe)樣(yang)品(pin)帶(dai)有(you)靜(jing)電(dian)。靜(jing)電(dian)現(xian)象(xiang)的(de)影(ying)響(xiang)將(jiang)使(shi)每(mei)次(ci)稱(cheng)量(liang)時(shi)稱(cheng)重(zhong)容(rong)器(qi)均(jun)顯(xian)示(shi)不(bu)同(tong)的(de)重(zhong)量(liang),結(jie)果(guo)的(de)重(zhong)複(fu)性(xing)很(hen)差(cha)。具(ju)有(you)高(gao)絕(jue)緣(yuan)度(du)的(de)材(cai)料(liao)如(ru)玻(bo)璃(li)、塑su料liao製zhi的de稱cheng重zhong容rong器qi等deng容rong易yi帶dai靜jing電dian。這zhe種zhong帶dai電dian現xian象xiang主zhu要yao是shi由you於yu樣yang品pin或huo容rong器qi在zai搬ban運yun過guo程cheng中zhong攪jiao拌ban或huo摩mo擦ca產chan生sheng的de,而er且qie一yi旦dan帶dai電dian則ze排pai除chu電dian荷he會hui非fei常chang緩huan慢man,在zai相xiang對dui濕shi度du低di於yu40%的(de)幹(gan)燥(zao)空(kong)氣(qi)中(zhong)出(chu)現(xian)樣(yang)品(pin)或(huo)容(rong)器(qi)帶(dai)靜(jing)電(dian)的(de)幾(ji)率(lv)會(hui)增(zeng)加(jia)。通(tong)常(chang)可(ke)采(cai)用(yong)打(da)開(kai)加(jia)濕(shi)器(qi)或(huo)適(shi)當(dang)調(tiao)節(jie)空(kong)調(tiao)係(xi)統(tong)來(lai)增(zeng)加(jia)空(kong)氣(qi)濕(shi)度(du),把(ba)稱(cheng)重(zhong)容(rong)器(qi)放(fang)在(zai)金(jin)屬(shu)容(rong)器(qi)內(nei)再(zai)進(jin)行(xing)稱(cheng)量(liang),設(she)法(fa)給(gei)分(fen)析(xi)天(tian)平(ping)接(jie)地(di)等(deng)措(cuo)施(shi),來(lai)去(qu)除(chu)或(huo)屏(ping)蔽(bi)稱(cheng)重(zhong)樣(yang)品(pin)上(shang)的(de)靜(jing)電(dian)。
4.使用者操作不當造成稱量不準確
稱量前沒有檢查,盲目稱量。稱量前應檢查天平是否正常,天平是否水平,稱盤是否潔淨、顯示屏是否歸零“000”位等。
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