實shi驗yan室shi的de儀yi器qi設she備bei是shi我wo們men的de工gong作zuo搭da檔dang,良liang好hao的de使shi用yong和he維wei護hu習xi慣guan,可ke以yi使shi我wo們men實shi驗yan更geng得de心xin應ying手shou,那na麼me具ju體ti這zhe些xie設she備bei應ying該gai如ru何he維wei護hu呢ne,一yi起qi看kan看吧。
電子天平
dianzitianpingshiwomendeshiyanzhongbibeidechenglianggongju,dabufenshiyanrenyuanyejibennengzhangwoqishiyongfangfa,danshiyandexijiehedasaoweihuzuodehenbudaowei,shiyanhouchengpanxiacanliuyouyixiewuzhi,chengpanshangliuyouwuzi。shitianpingdelingminduhezhunqueduxiajiang,shiyongshoumingyesuoduan。dianzitianpingshiyongqianxuxianyure10分鍾,但部分實驗人員開機後直接稱量。
稱cheng量liang物wu的de溫wen度du必bi須xu與yu天tian平ping溫wen度du相xiang同tong,不bu能neng把ba過guo熱re或huo過guo冷leng的de物wu體ti放fang在zai天tian平ping秤cheng盤pan上shang。一yi些xie具ju有you揮hui發fa性xing的de腐fu蝕shi性xing的de試shi劑ji應ying放fang在zai密mi閉bi容rong器qi中zhong稱cheng量liang,稱cheng量liang物wu體ti時shi要yao切qie記ji關guan閉bi天tian平ping的de側ce門men,稱cheng量liang完wan畢bi後hou及ji時shi打da掃sao稱cheng量liang盤pan上shang下xia及ji各ge個ge角jiao落luo等deng。
在空氣潮濕,物質已結成垢塊時,應采用機械除鏽方法,即先用鏟、剔、刮等方式將零部件上的鏽蝕層塊除去,再用砂紙砂磨、打光,最後塗上保護層。實驗完畢,關閉側門,蓋上天平布,置於避光幹燥處保存。
電熱恒溫幹燥箱
電熱恒溫幹燥箱是化學實驗中用於對物品進行烘焙、幹燥的常規儀器。幹燥箱的工作電壓為220V,溫度為100~110度(du),不(bu)宜(yi)過(guo)高(gao)。可(ke)燃(ran)性(xing)和(he)揮(hui)發(fa)性(xing)的(de)化(hua)學(xue)物(wu)品(pin)切(qie)勿(wu)放(fang)入(ru)箱(xiang)內(nei),箱(xiang)內(nei)載(zai)物(wu)應(ying)擺(bai)放(fang)應(ying)在(zai)隔(ge)板(ban)的(de)較(jiao)中(zhong)心(xin)部(bu)位(wei),同(tong)時(shi)不(bu)影(ying)響(xiang)空(kong)氣(qi)流(liu)通(tong)以(yi)保(bao)證(zheng)箱(xiang)內(nei)溫(wen)度(du)均(jun)勻(yun)。
幹燥箱使用過程中,學生不能用濕手觸摸箱體和開關。幹燥箱正常運行時如在使用過程中出現異常、氣味、煙yan霧wu等deng情qing況kuang,應ying立li即ji關guan閉bi電dian源yuan,請qing專zhuan業ye人ren員yuan查zha看kan修xiu理li。箱xiang壁bi內nei膽dan和he設she備bei表biao麵mian要yao經jing常chang擦ca拭shi,以yi保bao持chi清qing潔jie,增zeng加jia玻bo璃li的de透tou明ming度du。幹gan燥zao箱xiang若ruo長chang期qi不bu用yong,應ying拔ba掉diao電dian源yuan線xian以yi防fang止zhi設she備bei損sun傷shang人ren,並bing應ying定ding期qi按an使shi用yong條tiao件jian運yun行xing2~3天,以驅除電器部分的潮氣,避免損壞有關器件。
恒溫水浴鍋
恒溫水浴鍋主要用於實驗室中蒸餾,幹燥,濃縮化學藥品,也可用於恒溫加熱和其它溫度試驗,是化學實驗室、分析室、教(jiao)育(yu)科(ke)研(yan)的(de)必(bi)備(bei)工(gong)具(ju)。在(zai)使(shi)用(yong)中(zhong)學(xue)生(sheng)應(ying)該(gai)知(zhi)道(dao)它(ta)的(de)使(shi)用(yong)方(fang)法(fa)及(ji)注(zhu)意(yi)事(shi)項(xiang),以(yi)便(bian)實(shi)驗(yan)能(neng)夠(gou)順(shun)利(li)進(jin)行(xing)。加(jia)水(shui)之(zhi)前(qian)切(qie)勿(wu)接(jie)通(tong)電(dian)源(yuan),最(zui)好(hao)加(jia)入(ru)蒸(zheng)餾(liu)水(shui),以(yi)免(mian)產(chan)生(sheng)水(shui)垢(gou),加(jia)水(shui)不(bu)要(yao)太(tai)多(duo),以(yi)免(mian)沸(fei)騰(teng)時(shi)水(shui)量(liang)溢(yi)出(chu)鍋(guo)外(wai);鍋內水量也不可低於二分之一,不能使加熱管露出水麵;切qie勿wu無wu水shui或huo水shui位wei低di於yu隔ge板ban加jia熱re,否fou則ze會hui損sun壞huai加jia熱re管guan。注zhu水shui時shi不bu能neng將jiang水shui流liu入ru控kong製zhi箱xiang內nei,以yi防fang發fa生sheng觸chu電dian。如ru恒heng溫wen控kong製zhi失shi靈ling,可ke將jiang控kong製zhi器qi上shang的de銀yin接jie點dian用yong細xi砂sha布bu擦ca亮liang。使shi用yong完wan畢bi後hou,取qu出chu恒heng溫wen物wu,關guan閉bi電dian源yuan,排pai除chu箱xiang體ti內nei的de水shui,做zuo好hao儀yi器qi使shi用yong記ji錄lu。
燒杯
燒杯因其口徑上下一致,是取用液體、配製溶液、做(zuo)簡(jian)單(dan)化(hua)學(xue)反(fan)應(ying)最(zui)常(chang)用(yong)的(de)反(fan)應(ying)容(rong)器(qi)。但(dan)燒(shao)杯(bei)不(bu)能(neng)代(dai)替(ti)量(liang)筒(tong)量(liang)取(qu)液(ye)體(ti)。燒(shao)杯(bei)加(jia)熱(re)時(shi)要(yao)墊(dian)上(shang)石(shi)棉(mian)網(wang)。不(bu)能(neng)用(yong)火(huo)焰(yan)直(zhi)接(jie)加(jia)熱(re)燒(shao)杯(bei)。因(yin)為(wei)燒(shao)杯(bei)底(di)麵(mian)大(da),用(yong)火(huo)焰(yan)直(zhi)接(jie)加(jia)熱(re),隻(zhi)可(ke)燒(shao)到(dao)局(ju)部(bu),使(shi)玻(bo)璃(li)受(shou)熱(re)不(bu)勻(yun)而(er)引(yin)起(qi)炸(zha)裂(lie)。用(yong)燒(shao)杯(bei)加(jia)熱(re)液(ye)體(ti)時(shi),液(ye)體(ti)的(de)量(liang)以(yi)不(bu)超(chao)過(guo)燒(shao)杯(bei)容(rong)積(ji)的(de)1/3為(wei)宜(yi),以(yi)防(fang)沸(fei)騰(teng)時(shi)液(ye)體(ti)外(wai)溢(yi)。加(jia)熱(re)時(shi),燒(shao)杯(bei)外(wai)壁(bi)須(xu)擦(ca)幹(gan)。加(jia)熱(re)腐(fu)蝕(shi)性(xing)藥(yao)品(pin)時(shi),可(ke)將(jiang)一(yi)表(biao)麵(mian)皿(min)蓋(gai)在(zai)燒(shao)杯(bei)口(kou)上(shang),以(yi)免(mian)液(ye)體(ti)濺(jian)出(chu)。不(bu)可(ke)用(yong)燒(shao)杯(bei)長(chang)期(qi)盛(sheng)放(fang)化(hua)學(xue)藥(yao)品(pin),以(yi)免(mian)落(luo)入(ru)塵(chen)土(tu)和(he)使(shi)溶(rong)液(ye)中(zhong)的(de)水(shui)分(fen)蒸(zheng)發(fa)。溶(rong)解(jie)或(huo)稀(xi)釋(shi)過(guo)程(cheng)中(zhong),用(yong)玻(bo)璃(li)棒(bang)攪(jiao)拌(ban)時(shi),不(bu)要(yao)觸(chu)及(ji)杯(bei)底(di)或(huo)杯(bei)壁(bi)。
試管
實驗室用來盛放少量藥品,加熱情況下少量試劑反應的容器。裝溶液時不超過試管容量的1/2,加熱時不超過試管的1/3。取塊狀固體放入試管要用鑷子,不能使固體直接墜入試管中,防止試管底破裂。加熱時使用試管夾,試管夾應夾在距管口1/3處。試管口不能對著人。試管不可以直接加熱,要先預熱,加熱盛有固體的試管時,管口略向下,加熱液體時傾斜約45°。加(jia)熱(re)時(shi)要(yao)保(bao)持(chi)試(shi)管(guan)外(wai)壁(bi)沒(mei)有(you)水(shui)珠(zhu),防(fang)止(zhi)受(shou)熱(re)不(bu)均(jun)勻(yun)而(er)爆(bao)裂(lie)。加(jia)熱(re)後(hou)不(bu)能(neng)驟(zhou)冷(leng),防(fang)止(zhi)試(shi)管(guan)破(po)裂(lie)。加(jia)熱(re)後(hou)不(bu)能(neng)在(zai)試(shi)管(guan)未(wei)冷(leng)卻(que)至(zhi)室(shi)溫(wen)時(shi)就(jiu)洗(xi)滌(di)試(shi)管(guan)。加(jia)熱(re)時(shi)應(ying)用(yong)外(wai)焰(yan)。
容量瓶
容rong量liang瓶ping主zhu要yao用yong於yu準zhun確que地di配pei製zhi一yi定ding摩mo爾er濃nong度du的de溶rong液ye,它ta是shi一yi種zhong細xi長chang頸jing,梨li形xing的de平ping底di玻bo璃li瓶ping,帶dai有you磨mo口kou玻bo璃li塞sai,瓶ping頸jing上shang刻ke有you標biao線xian,當dang瓶ping內nei液ye體ti在zai所suo指zhi定ding溫wen度du下xia達da到dao標biao線xian處chu時shi,其qi體ti積ji即ji為wei瓶ping上shang所suo注zhu明ming的de容rong積ji數shu。
rongliangpingbunengpeizhiqirongjiyixiatijiderongye,jiqirongjiweiduoda,jiuzhinengpeizhiduodatijiderongye。rongliangpingshiyongqianyingxianjianzhashifouloushui,yiciyongzilaishui,zhengliushuixihaobeiyong。jiangrongzhizaishaobeizhongrongjiehouzhuanyidaorongliangpingli,bunengzairongliangpinglijinxingrongzhiderongjie,kongzhirongjierongzhidezhengliushuiliang。
轉zhuan移yi時shi必bi須xu用yong玻bo璃li棒bang引yin流liu。容rong量liang瓶ping不bu能neng進jin行xing加jia熱re,如ru果guo溶rong質zhi在zai溶rong解jie過guo程cheng中zhong放fang熱re,要yao待dai溶rong液ye冷leng卻que後hou再zai進jin行xing轉zhuan移yi,因yin為wei溫wen度du升sheng高gao瓶ping體ti將jiang膨peng脹zhang,所suo量liang體ti積ji就jiu會hui不bu準zhun確que。用yong於yu洗xi滌di燒shao杯bei的de溶rong劑ji總zong量liang不bu能neng超chao過guo容rong量liang瓶ping的de標biao線xian,一yi旦dan超chao過guo,必bi須xu重zhong新xin進jin行xing配pei置zhi。
peizhihaoderongyezhuanyizhishijipingzhongbaocun,rongliangpingzhinengpeizhirongye,bunengchucunrongye,yinweirongyekenenghuiduipingtijinxingfushi,congershirongliangpingdejingdushoudaoyingxiang。rongliangpingshiyongwanbiyingjishiyongshuichongxiganjing,saishangpingsai,bingzaisaiziyupingkouzhijianjiayitiaozhitiao,fangzhipingsaiyupingkouzhanlian。zuihoujilurongyetijideshihouyibanbaoliu4位有效數字(XXX.0mL)。
滴定管
滴定管是可放出不固定量液體的量出式玻璃儀器,主要用於滴定分析中對滴定劑體積的測量。能精確到到0.01mL。帶玻璃活塞的滴定管為酸式滴定管,帶有內裝玻璃球的橡皮管的滴定管為堿式滴定管。酸式、堿式滴定管不能混用,酸式滴定管裝酸性物質和大多數中性物質(尤其是強氧化劑),堿式滴定管裝堿性物質(包括堿和堿性鹽),滴定管使用前先檢查是否漏液,如果漏水,應重新將活塞塗凡士林油。裝液前要用洗液、水依次衝洗幹淨,並要用待裝的溶液潤洗滴定管。
將(jiang)操(cao)作(zuo)溶(rong)液(ye)倒(dao)入(ru),直(zhi)到(dao)充(chong)滿(man)至(zhi)零(ling)刻(ke)度(du)線(xian)以(yi)上(shang)為(wei)止(zhi)。注(zhu)意(yi)檢(jian)查(zha)滴(di)定(ding)管(guan)的(de)出(chu)口(kou)管(guan)是(shi)否(fou)充(chong)滿(man)溶(rong)液(ye),如(ru)有(you)氣(qi)泡(pao)進(jin)行(xing)排(pai)氣(qi)泡(pao)操(cao)作(zuo)。調(tiao)整(zheng)液(ye)麵(mian)時(shi),使(shi)液(ye)麵(mian)保(bao)持(chi)在(zai)“0”或“0”yixiademouyidingkedu。jinxingdidingshi,yingjiangdidingguanchuizhidijiazaididingguanjiashang,rushiyongdeshijianshididingguan,muzhiyushizhizaibolizhusuozaibuweiyipangnierujiaoguan,buyaoniebolizhu,yebunengshiqishangxiayidong。didingshiyingzhudilianxudijia,jiejinzhongdianshi,zhijiayidihuobandi,zhirongyechuxianmingxiandeyansebianhua。
讀數時,手拿滴定管上部無刻度處,使滴定管保持垂直,視線平視溶液的凹液麵,讀到小數點後第二位,即估計到0.01mL。滴定結束後,管內剩餘的溶液應棄去,不得將其倒回原瓶,隨即清洗滴定管,並倒掛於鐵架台上。
常用玻璃儀器的洗滌
實驗室常用的玻璃儀器如燒杯、試管、滴定管、移液管、容量瓶等。儀器在使用中會沾上油汙,水垢,鏽跡等,使用後不及時完全的清洗,會造成結果誤差,甚至會對儀器的壽命、性能會產生極其不良的影響。因此,化學實驗使用的玻璃儀器必須洗滌幹淨。下麵介紹一些玻璃儀器的洗滌方法。
附(fu)有(you)易(yi)去(qu)除(chu)物(wu)質(zhi)的(de)簡(jian)單(dan)儀(yi)器(qi),如(ru)試(shi)管(guan)。燒(shao)杯(bei)等(deng),先(xian)用(yong)自(zi)來(lai)水(shui)衝(chong)洗(xi),再(zai)用(yong)試(shi)管(guan)刷(shua)蘸(zhan)取(qu)合(he)成(cheng)洗(xi)滌(di)劑(ji)刷(shua)洗(xi),最(zui)後(hou)自(zi)來(lai)水(shui)衝(chong)洗(xi)。當(dang)倒(dao)置(zhi)儀(yi)器(qi),器(qi)壁(bi)形(xing)成(cheng)一(yi)層(ceng)均(jun)勻(yun)的(de)水(shui)膜(mo),不(bu)成(cheng)股(gu)流(liu)下(xia)時(shi),即(ji)已(yi)洗(xi)淨(jing)。有(you)油(you)汙(wu)的(de)玻(bo)璃(li)器(qi)皿(min),先(xian)用(yong)堿(jian)性(xing)酒(jiu)精(jing)洗(xi)滌(di)液(ye)洗(xi)滌(di),然(ran)後(hou)用(yong)洗(xi)衣(yi)粉(fen)水(shui)或(huo)肥(fei)皂(zao)水(shui)洗(xi)滌(di),再(zai)用(yong)自(zi)來(lai)水(shui)衝(chong)洗(xi)幹(gan)淨(jing)。有(you)鏽(xiu)跡(ji),水(shui)垢(gou)的(de)器(qi)皿(min),用(yong)(1+3)鹽(yan)酸(suan)洗(xi)液(ye)浸(jin)泡(pao),再(zai)用(yong)再(zai)來(lai)水(shui)衝(chong)洗(xi)幹(gan)淨(jing)。有(you)凡(fan)士(shi)林(lin)油(you)汙(wu)的(de)器(qi)皿(min),先(xian)將(jiang)凡(fan)士(shi)林(lin)擦(ca)去(qu),再(zai)用(yong)洗(xi)衣(yi)粉(fen)水(shui)或(huo)肥(fei)皂(zao)水(shui)洗(xi)燒(shao)煮(zhu),取(qu)出(chu)後(hou)用(yong)自(zi)來(lai)水(shui)衝(chong)洗(xi)幹(gan)淨(jing)。一(yi)些(xie)構(gou)造(zao)比(bi)較(jiao)精(jing)細(xi)、複雜的玻璃儀器,如容量瓶、移液管等,無法用毛刷刷洗,可以用洗滌液浸泡一定時間,再進行清洗。洗淨的玻璃儀器不要再用手、布或紙擦拭,以免重新汙染。
常用光學儀器的維護與清洗
實驗室常用的光學儀器如分光光度計、折光計的棱鏡、玻片等,都是一些精密光學儀器,在使用和保養中,必須細心謹慎,嚴格按說明使用,不得任意鬆動儀器各連接部分,不得跌落、碰(peng)撞(zhuang)儀(yi)器(qi),以(yi)防(fang)止(zhi)光(guang)學(xue)零(ling)件(jian)損(sun)傷(shang)及(ji)影(ying)響(xiang)精(jing)度(du)。被(bei)測(ce)試(shi)樣(yang)中(zhong)不(bu)應(ying)有(you)硬(ying)性(xing)雜(za)質(zhi),當(dang)測(ce)試(shi)固(gu)體(ti)試(shi)樣(yang)時(shi),應(ying)防(fang)止(zhi)把(ba)折(zhe)射(she)棱(leng)鏡(jing)表(biao)麵(mian)拉(la)毛(mao)或(huo)產(chan)生(sheng)壓(ya)痕(hen)。使(shi)用(yong)完(wan)畢(bi)後(hou),嚴(yan)禁(jin)直(zhi)接(jie)放(fang)入(ru)水(shui)中(zhong)清(qing)洗(xi),避(bi)免(mian)光(guang)學(xue)係(xi)統(tong)管(guan)路(lu)進(jin)水(shui)。打(da)開(kai)棱(leng)鏡(jing),用(yong)擦(ca)鏡(jing)紙(zhi)輕(qing)輕(qing)擦(ca)幹(gan),不(bu)論(lun)在(zai)任(ren)何(he)情(qing)況(kuang)下(xia),不(bu)允(yun)許(xu)用(yong)擦(ca)鏡(jing)紙(zhi)以(yi)外(wai)的(de)任(ren)何(he)東(dong)西(xi)接(jie)觸(chu)到(dao)棱(leng)鏡(jing),以(yi)免(mian)損(sun)壞(huai)它(ta)的(de)光(guang)學(xue)平(ping)麵(mian)。儀(yi)器(qi)應(ying)存(cun)放(fang)於(yu)幹(gan)燥(zao)、無灰塵、無油汙和無有害、易燃、易爆等氣體的地方,以免光學零件腐蝕或生黴。光學儀器在使用中容易沾上油汙、水濕性汙物、指紋等,影響成像及透光率。清洗折光計的棱鏡、平麵鏡、xianweijingdejingtou,xianyongzhengliushuijinxingqingxi,jingmianruoyouwuzi,keyiyongyichunheyimidehunheyeqingxi。qingxishiyongzhuanmendecajingzhihuomianqiuzhanyoushaoliangqingxiji,shunzheyigefangxiangcashi,congjingtouzhongxinxiangwaizuoyuanyundong,qiejibazheleijingtoujinpaozaiqingxijizhongqingxi。qingxijingtoubudeyonglishica,fouzehuihuashangzengtoumo,sunhuaijingtou。qingxiwanbihouyongcajingzhicagan,biguangbaocun。
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