1.分析天平在使用前沒有經過校準
一(yi)台(tai)分(fen)析(xi)天(tian)平(ping)在(zai)使(shi)用(yong)之(zhi)前(qian),首(shou)先(xian)要(yao)確(que)認(ren)它(ta)的(de)正(zheng)確(que)性(xing)是(shi)否(fou)合(he)格(ge),否(fou)則(ze)該(gai)天(tian)平(ping)所(suo)稱(cheng)量(liang)的(de)正(zheng)確(que)性(xing)得(de)不(bu)到(dao)保(bao)證(zheng)。分(fen)析(xi)天(tian)平(ping)從(cong)首(shou)次(ci)使(shi)用(yong)起(qi),應(ying)對(dui)其(qi)定(ding)期(qi)校(xiao)準(zhun)。連(lian)續(xu)使(shi)用(yong)的(de)天(tian)平(ping),大(da)約(yue)每(mei)星(xing)期(qi)校(xiao)準(zhun)一(yi)次(ci)。校(xiao)準(zhun)時(shi)應(ying)按(an)規(gui)定(ding)程(cheng)序(xu)進(jin)行(xing),必(bi)須(xu)使(shi)用(yong)標(biao)準(zhun)砝(fa)碼(ma)進(jin)行(xing)校(xiao)準(zhun),否(fou)則(ze)將(jiang)起(qi)不(bu)到(dao)校(xiao)準(zhun)的(de)作(zuo)用(yong)。
2.分析天平安裝不正確
在安裝分析天平時首先要選擇選防塵、防潮、防震、防風、防曬、hengwendefangjianzuoweitianpingshi。qici,tianpingyinganfangzailaogukekaodegongzuotaishang,bingxuanzeshidangdeweizhianfang。tianpinganzhuangqian,yinganzhuangxiangqingdanjinxingqingdian,kangebujianshifouqiquan、完(wan)好(hao),並(bing)對(dui)天(tian)平(ping)的(de)所(suo)有(you)部(bu)件(jian)進(jin)行(xing)仔(zai)細(xi)清(qing)潔(jie)。安(an)裝(zhuang)時(shi),應(ying)參(can)照(zhao)天(tian)平(ping)的(de)說(shuo)明(ming)書(shu)正(zheng)確(que)裝(zhuang)配(pei)天(tian)平(ping)。安(an)裝(zhuang)完(wan)畢(bi)後(hou)應(ying)再(zai)次(ci)檢(jian)查(zha)各(ge)部(bu)分(fen)安(an)裝(zhuang)是(shi)否(fou)正(zheng)常(chang),然(ran)後(hou)檢(jian)查(zha)電(dian)源(yuan)電(dian)壓(ya)是(shi)否(fou)符(fu)合(he)天(tian)平(ping)的(de)要(yao)求(qiu),打(da)開(kai)天(tian)平(ping)檢(jian)查(zha)是(shi)否(fou)正(zheng)常(chang)。
3.環境及樣品的物理因素影響
在使用分析天平進行稱量的過程中,環境和物理因素會對稱量結果產生幹擾,如溫度、樣品揮發、吸濕、磁力、靜電等的幹擾。
(1)溫度的變化對分析天平的影響
如(ru)果(guo)在(zai)稱(cheng)量(liang)過(guo)程(cheng)中(zhong)發(fa)現(xian)顯(xian)示(shi)值(zhi)單(dan)方(fang)向(xiang)漂(piao)移(yi),就(jiu)有(you)可(ke)能(neng)是(shi)溫(wen)度(du)變(bian)化(hua)所(suo)產(chan)生(sheng)的(de)影(ying)響(xiang)。若(ruo)樣(yang)品(pin)與(yu)周(zhou)圍(wei)環(huan)境(jing)之(zhi)間(jian)的(de)溫(wen)度(du)存(cun)在(zai)差(cha)異(yi),則(ze)這(zhe)個(ge)溫(wen)度(du)差(cha)異(yi)就(jiu)會(hui)導(dao)致(zhi)沿(yan)稱(cheng)重(zhong)容(rong)器(qi)流(liu)動(dong)的(de)氣(qi)流(liu)。空(kong)氣(qi)沿(yan)著(zhe)容(rong)器(qi)外(wai)側(ce)流(liu)動(dong)產(chan)生(sheng)一(yi)個(ge)向(xiang)上(shang)的(de)作(zuo)用(yong)力(li),這(zhe)個(ge)力(li)就(jiu)導(dao)致(zhi)稱(cheng)重(zhong)結(jie)果(guo)產(chan)生(sheng)錯(cuo)誤(wu):yangpinzaidongtaifulizuoyongxia,chengdedezhongliangbishijiyaoqing。zhegezuoyongzhidaowendupinghengxingchengyihoucaihuizhongzhi。dangbayangpincongganzaoluhuobingxiangzhongquchuyihou,yaodengdaoyangpinwenduyushiyanshihuochengliangshiwenduyizhishicaikeyichengliang。yangpinyaofangzaibiaomianjijinkenengxiaodequpirongqizhong,qufangchengliangrongqiyaoshiyongniezijiaqu,erbunengjiangshoufangruchengliangshizhong。
(2)樣品吸濕或揮發對稱量結果的影響
如果在稱量的過程中顯示值單方向持續漂移,則可能測量的是揮發性或吸濕性樣品。若樣品吸濕性較強,則重量會增大;ruobeiceliangyangpinshuyihuifawuzhi,zezhonglianghuijianxiao。duiyuxishixinghuohuifaxingyangpinkeshiyongxijingrongqi,geirongqijiagaihuoshangsai,shiyongqingjieganzaodechengzhongrongqibingbaochichengpanshangbuzhanyouhuichen、汙染物及水滴。
(3)樣品或容器帶靜電對稱量結果的影響
如ru果guo每mei次ci稱cheng量liang都dou顯xian示shi不bu同tong的de稱cheng量liang結jie果guo或huo顯xian示shi值zhi不bu穩wen定ding,或huo稱cheng量liang結jie果guo的de重zhong複fu性xing差cha,則ze可ke考kao慮lv是shi稱cheng量liang容rong器qi或huo者zhe樣yang品pin帶dai有you靜jing電dian。靜jing電dian現xian象xiang的de影ying響xiang將jiang使shi每mei次ci稱cheng量liang時shi稱cheng重zhong容rong器qi均jun顯xian示shi不bu同tong的de重zhong量liang,結jie果guo的de重zhong複fu性xing很hen差cha。具ju有you高gao絕jue緣yuan度du的de材cai料liao如ru玻bo璃li、塑(su)料(liao)製(zhi)的(de)稱(cheng)重(zhong)容(rong)器(qi)等(deng)容(rong)易(yi)帶(dai)靜(jing)電(dian)。這(zhe)種(zhong)帶(dai)電(dian)現(xian)象(xiang)主(zhu)要(yao)是(shi)由(you)於(yu)樣(yang)品(pin)或(huo)容(rong)器(qi)在(zai)搬(ban)運(yun)過(guo)程(cheng)中(zhong)攪(jiao)拌(ban)或(huo)摩(mo)擦(ca)產(chan)生(sheng)的(de),而(er)且(qie)一(yi)旦(dan)帶(dai)電(dian)則(ze)排(pai)除(chu)電(dian)荷(he)會(hui)非(fei)常(chang)緩(huan)慢(man),在(zai)相(xiang)對(dui)濕(shi)度(du)低(di)於(yu)40%的(de)幹(gan)燥(zao)空(kong)氣(qi)中(zhong)出(chu)現(xian)樣(yang)品(pin)或(huo)容(rong)器(qi)帶(dai)靜(jing)電(dian)的(de)幾(ji)率(lv)會(hui)增(zeng)加(jia)。通(tong)常(chang)可(ke)采(cai)用(yong)打(da)開(kai)加(jia)濕(shi)器(qi)或(huo)適(shi)當(dang)調(tiao)節(jie)空(kong)調(tiao)係(xi)統(tong)來(lai)增(zeng)加(jia)空(kong)氣(qi)濕(shi)度(du),把(ba)稱(cheng)重(zhong)容(rong)器(qi)放(fang)在(zai)金(jin)屬(shu)容(rong)器(qi)內(nei)再(zai)進(jin)行(xing)稱(cheng)量(liang),設(she)法(fa)給(gei)分(fen)析(xi)天(tian)平(ping)接(jie)地(di)等(deng)措(cuo)施(shi),來(lai)去(qu)除(chu)或(huo)屏(ping)蔽(bi)稱(cheng)重(zhong)樣(yang)品(pin)上(shang)的(de)靜(jing)電(dian)。
4.使用者操作不當造成稱量不準確
稱量前沒有檢查,盲目稱量。稱量前應檢查天平是否正常,天平是否水平,稱盤是否潔淨、顯示屏是否歸零“000”位等等。
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