恒溫水浴鍋、燒杯等玻璃儀器怎麼保養?

發布日期:2024-08-28
核心提示:恒溫水浴鍋恒溫水浴鍋主要用於實驗室中蒸餾,幹燥,濃縮化學藥品,也可用於恒溫加熱和其它溫度試驗,是化學實驗室、分析室、教育

恒溫水浴鍋主要用於實驗室中蒸餾,幹燥,濃縮化學藥品,也可用於恒溫加熱和其它溫度試驗,是化學實驗室、分析室、教育科研的必備工具。在zai使shi用yong中zhong學xue生sheng應ying該gai知zhi道dao它ta的de使shi用yong方fang法fa及ji注zhu意yi事shi項xiang,以yi便bian實shi驗yan能neng夠gou順shun利li進jin行xing。加jia水shui之zhi前qian切qie勿wu接jie通tong電dian源yuan,最zui好hao加jia入ru蒸zheng餾liu水shui,以yi免mian產chan生sheng水shui垢gou,加jia水shui不bu要yao太tai多duo,以yi免mian沸fei騰teng時shi水shui量liang溢yi出chu鍋guo外wai;鍋內水量也不可低於二分之一,不能使加熱管露出水麵;切qie勿wu無wu水shui或huo水shui位wei低di於yu隔ge板ban加jia熱re,否fou則ze會hui損sun壞huai加jia熱re管guan。注zhu水shui時shi不bu能neng將jiang水shui流liu入ru控kong製zhi箱xiang內nei,以yi防fang發fa生sheng觸chu電dian。如ru恒heng溫wen控kong製zhi失shi靈ling,可ke將jiang控kong製zhi器qi上shang的de銀yin接jie點dian用yong細xi砂sha布bu擦ca亮liang。使shi用yong完wan畢bi後hou,取qu出chu恒heng溫wen物wu,關guan閉bi電dian源yuan,排pai除chu箱xiang體ti內nei的de水shui,做zuo好hao儀yi器qi使shi用yong記ji錄lu。燒杯因其口徑上下一致,是取用液體、配製溶液、做簡單化學反應最常用的反應容器。但燒杯不能代替量筒量取液體。燒杯加熱時要墊上石棉網。不能用火焰直接加熱燒杯。因為燒杯底麵大,用火焰直接加熱,隻可燒到局部,使玻璃受熱不勻而引起炸裂。用燒杯加熱液體時,液體的量以不超過燒杯容積的1/3為wei宜yi,以yi防fang沸fei騰teng時shi液ye體ti外wai溢yi。加jia熱re時shi,燒shao杯bei外wai壁bi須xu擦ca幹gan。加jia熱re腐fu蝕shi性xing藥yao品pin時shi,可ke將jiang一yi表biao麵mian皿min蓋gai在zai燒shao杯bei口kou上shang,以yi免mian液ye體ti濺jian出chu。不bu可ke用yong燒shao杯bei長chang期qi盛sheng放fang化hua學xue藥yao品pin,以yi免mian落luo入ru塵chen土tu和he使shi溶rong液ye中zhong的de水shui分fen蒸zheng發fa。溶rong解jie或huo稀xi釋shi過guo程cheng中zhong,用yong玻bo璃li棒bang攪jiao拌ban時shi,不bu要yao觸chu及ji杯bei底di或huo杯bei壁bi。實驗室用來盛放少量藥品,加熱情況下少量試劑反應的容器。裝溶液時不超過試管容量的1/2,加熱時不超過試管的1/3。取塊狀固體放入試管要用鑷子,不能使固體直接墜入試管中,防止試管底破裂。加熱時使用試管夾,試管夾應夾在距管口1/3處。試管口不能對著人。試管不可以直接加熱,要先預熱,加熱盛有固體的試管時,管口略向下,加熱液體時傾斜約45°。jiareshiyaobaochishiguanwaibimeiyoushuizhu,fangzhishourebujunyunerbaolie。jiarehoubunengzhouleng,fangzhishiguanpolie。jiarehoubunengzaishiguanweilengquezhishiwenshijiuxidishiguan。jiareshiyingyongwaiyan。容量瓶主要用於準確地配製一定摩爾濃度derongye,tashiyizhongxichangjing,lixingdepingdiboliping,daiyoumokoubolisai,pingjingshangkeyoubiaoxian,dangpingneiyetizaisuozhidingwenduxiadadaobiaoxianchushi,qitijijiweipingshangsuozhumingderongjishu。容rong量liang瓶ping不bu能neng配pei製zhi其qi容rong積ji以yi下xia體ti積ji的de溶rong液ye,即ji其qi容rong積ji為wei多duo大da,就jiu隻zhi能neng配pei製zhi多duo大da體ti積ji的de溶rong液ye。容rong量liang瓶ping使shi用yong前qian應ying先xian檢jian查zha是shi否fou漏lou水shui,依yi次ci用yong自zi來lai水shui,蒸zheng餾liu水shui洗xi好hao備bei用yong。將jiang溶rong質zhi在zai燒shao杯bei中zhong溶rong解jie後hou轉zhuan移yi到dao容rong量liang瓶ping裏li,不bu能neng在zai容rong量liang瓶ping裏li進jin行xing溶rong質zhi的de溶rong解jie,控kong製zhi溶rong解jie溶rong質zhi的de蒸zheng餾liu水shui量liang。轉zhuan移yi時shi必bi須xu用yong玻bo璃li棒bang引yin流liu。容rong量liang瓶ping不bu能neng進jin行xing加jia熱re,如ru果guo溶rong質zhi在zai溶rong解jie過guo程cheng中zhong放fang熱re,要yao待dai溶rong液ye冷leng卻que後hou再zai進jin行xing轉zhuan移yi,因yin為wei溫wen度du升sheng高gao瓶ping體ti將jiang膨peng脹zhang,所suo量liang體ti積ji就jiu會hui不bu準zhun確que。用yong於yu洗xi滌di燒shao杯bei的de溶rong劑ji總zong量liang不bu能neng超chao過guo容rong量liang瓶ping的de標biao線xian,一yi旦dan超chao過guo,必bi須xu重zhong新xin進jin行xing配pei置zhi。配(pei)製(zhi)好(hao)的(de)溶(rong)液(ye)轉(zhuan)移(yi)至(zhi)試(shi)劑(ji)瓶(ping)中(zhong)保(bao)存(cun),容(rong)量(liang)瓶(ping)隻(zhi)能(neng)配(pei)製(zhi)溶(rong)液(ye),不(bu)能(neng)儲(chu)存(cun)溶(rong)液(ye),因(yin)為(wei)溶(rong)液(ye)可(ke)能(neng)會(hui)對(dui)瓶(ping)體(ti)進(jin)行(xing)腐(fu)蝕(shi),從(cong)而(er)使(shi)容(rong)量(liang)瓶(ping)的(de)精(jing)度(du)受(shou)到(dao)影(ying)響(xiang)。容(rong)量(liang)瓶(ping)使(shi)用(yong)完(wan)畢(bi)應(ying)及(ji)時(shi)用(yong)水(shui)衝(chong)洗(xi)幹(gan)淨(jing),塞(sai)上(shang)瓶(ping)塞(sai),並(bing)在(zai)塞(sai)子(zi)與(yu)瓶(ping)口(kou)之(zhi)間(jian)夾(jia)一(yi)條(tiao)紙(zhi)條(tiao),防(fang)止(zhi)瓶(ping)塞(sai)與(yu)瓶(ping)口(kou)粘(zhan)連(lian)。最(zui)後(hou)記(ji)錄(lu)溶(rong)液(ye)體(ti)積(ji)的(de)時(shi)候(hou)一(yi)般(ban)保(bao)留(liu)4位有效數字(XXX.0mL)。滴定管是可放出不固定量液體的量出式玻璃儀器,主要用於滴定分析中對滴定劑體積的測量。能精確到到0.01mL。帶玻璃活塞的滴定管為酸式滴定管,帶有內裝玻璃球的橡皮管的滴定管為堿式滴定管。酸式、堿式滴定管不能混用,酸式滴定管裝酸性物質和大多數中性物質(尤其是強氧化劑),堿式滴定管裝堿性物質(包括堿和堿性鹽),滴定管使用前先檢查是否漏液,如果漏水,應重新將活塞塗凡士林油。裝液前要用洗液、水依次衝洗幹淨,並要用待裝的溶液潤洗滴定管。將(jiang)操(cao)作(zuo)溶(rong)液(ye)倒(dao)入(ru),直(zhi)到(dao)充(chong)滿(man)至(zhi)零(ling)刻(ke)度(du)線(xian)以(yi)上(shang)為(wei)止(zhi)。注(zhu)意(yi)檢(jian)查(zha)滴(di)定(ding)管(guan)的(de)出(chu)口(kou)管(guan)是(shi)否(fou)充(chong)滿(man)溶(rong)液(ye),如(ru)有(you)氣(qi)泡(pao)進(jin)行(xing)排(pai)氣(qi)泡(pao)操(cao)作(zuo)。調(tiao)整(zheng)液(ye)麵(mian)時(shi),使(shi)液(ye)麵(mian)保(bao)持(chi)在(zai)“0”或“0”以下的某一定刻度。進行滴定時,應將滴定管垂直地夾在滴定管夾上,如使用的是堿式滴定管,拇指與食指在玻璃珠所在部位一旁捏乳膠管,不要捏玻璃珠,也不能使其上下移動。滴定時應逐滴連續滴加,接近終點時,隻加一滴或半滴,至溶液出現明顯的顏色變化。讀數時,手拿滴定管上部無刻度處,使滴定管保持垂直,視線平視溶液的凹液麵,讀到小數點後第二位,即估計到0.01mL。滴定結束後,管內剩餘的溶液應棄去,不得將其倒回原瓶,隨即清洗滴定管,並倒掛於鐵架台上。
編輯:songjiajie2010