shiyanshideyiqishebeishiwomendegongzuodadang,lianghaodeshiyongheweihuxiguan,keyishiwomenshiyangengdexinyingshou,namejutizhexieshebeiyinggairuheweihune,xiaohuobanmenyiqilaikankanba。電(dian)子(zi)天(tian)平(ping)是(shi)我(wo)們(men)的(de)實(shi)驗(yan)中(zhong)必(bi)備(bei)的(de)稱(cheng)量(liang)工(gong)具(ju),大(da)部(bu)分(fen)實(shi)驗(yan)人(ren)員(yuan)也(ye)基(ji)本(ben)能(neng)掌(zhang)握(wo)其(qi)使(shi)用(yong)方(fang)法(fa),但(dan)實(shi)驗(yan)的(de)細(xi)節(jie)和(he)打(da)掃(sao)維(wei)護(hu)做(zuo)的(de)很(hen)不(bu)到(dao)位(wei),實(shi)驗(yan)後(hou)秤(cheng)盤(pan)下(xia)殘(can)留(liu)有(you)一(yi)些(xie)物(wu)質(zhi),秤(cheng)盤(pan)上(shang)留(liu)有(you)汙(wu)漬(zi)。使(shi)天(tian)平(ping)的(de)靈(ling)敏(min)度(du)和(he)準(zhun)確(que)度(du)下(xia)降(jiang),使(shi)用(yong)壽(shou)命(ming)也(ye)縮(suo)短(duan)。電(dian)子(zi)天(tian)平(ping)使(shi)用(yong)前(qian)須(xu)先(xian)預(yu)熱(re)10分鍾,但部分實驗人員開機後直接稱量。稱(cheng)量(liang)物(wu)的(de)溫(wen)度(du)必(bi)須(xu)與(yu)天(tian)平(ping)溫(wen)度(du)相(xiang)同(tong),不(bu)能(neng)把(ba)過(guo)熱(re)或(huo)過(guo)冷(leng)的(de)物(wu)體(ti)放(fang)在(zai)天(tian)平(ping)秤(cheng)盤(pan)上(shang)。一(yi)些(xie)具(ju)有(you)揮(hui)發(fa)性(xing)的(de)腐(fu)蝕(shi)性(xing)的(de)試(shi)劑(ji)應(ying)放(fang)在(zai)密(mi)閉(bi)容(rong)器(qi)中(zhong)稱(cheng)量(liang),稱(cheng)量(liang)物(wu)體(ti)時(shi)要(yao)切(qie)記(ji)關(guan)閉(bi)天(tian)平(ping)的(de)側(ce)門(men),稱(cheng)量(liang)完(wan)畢(bi)後(hou)及(ji)時(shi)打(da)掃(sao)稱(cheng)量(liang)盤(pan)上(shang)下(xia)及(ji)各(ge)個(ge)角(jiao)落(luo)等(deng)。在空氣潮濕,物質已結成垢塊時,應采用機械除鏽方法,即先用鏟、剔、刮等方式將零部件上的鏽蝕層塊除去,再用砂紙砂磨、打光,最後塗上保護層。實驗完畢,關閉側門,蓋上天平布,置於避光幹燥處保存。電熱恒溫幹燥箱是化學實驗中用於對物品進行烘焙、幹燥的常規儀器。幹燥箱的工作電壓為220V,溫度為100~110度du,不bu宜yi過guo高gao。可ke燃ran性xing和he揮hui發fa性xing的de化hua學xue物wu品pin切qie勿wu放fang入ru箱xiang內nei,箱xiang內nei載zai物wu應ying擺bai放fang應ying在zai隔ge板ban的de較jiao中zhong心xin部bu位wei,同tong時shi不bu影ying響xiang空kong氣qi流liu通tong以yi保bao證zheng箱xiang內nei溫wen度du均jun勻yun。幹燥箱使用過程中,學生不能用濕手觸摸箱體和開關。幹燥箱正常運行時如在使用過程中出現異常、氣味、yanwudengqingkuang,yinglijiguanbidianyuan,qingzhuanyerenyuanzhakanxiuli。xiangbineidanheshebeibiaomianyaojingchangcashi,yibaochiqingjie,zengjiabolidetoumingdu。ganzaoxiangruochangqibuyong,yingbadiaodianyuanxianyifangzhishebeisunshangren,bingyingdingqianshiyongtiaojianyunxing2~3天,以驅除電器部分的潮氣,避免損壞有關器件。恒溫水浴鍋主要用於實驗室中蒸餾,幹燥,濃縮化學藥品,也可用於恒溫加熱和其它溫度試驗,是化學實驗室、分析室、教育科研的必備工具。zaishiyongzhongxueshengyinggaizhidaotadeshiyongfangfajizhuyishixiang,yibianshiyannenggoushunlijinxing。jiashuizhiqianqiewujietongdianyuan,zuihaojiaruzhengliushui,yimianchanshengshuigou,jiashuibuyaotaiduo,yimianfeitengshishuiliangyichuguowai;鍋內水量也不可低於二分之一,不能使加熱管露出水麵;切(qie)勿(wu)無(wu)水(shui)或(huo)水(shui)位(wei)低(di)於(yu)隔(ge)板(ban)加(jia)熱(re),否(fou)則(ze)會(hui)損(sun)壞(huai)加(jia)熱(re)管(guan)。注(zhu)水(shui)時(shi)不(bu)能(neng)將(jiang)水(shui)流(liu)入(ru)控(kong)製(zhi)箱(xiang)內(nei),以(yi)防(fang)發(fa)生(sheng)觸(chu)電(dian)。如(ru)恒(heng)溫(wen)控(kong)製(zhi)失(shi)靈(ling),可(ke)將(jiang)控(kong)製(zhi)器(qi)上(shang)的(de)銀(yin)接(jie)點(dian)用(yong)細(xi)砂(sha)布(bu)擦(ca)亮(liang)。使(shi)用(yong)完(wan)畢(bi)後(hou),取(qu)出(chu)恒(heng)溫(wen)物(wu),關(guan)閉(bi)電(dian)源(yuan),排(pai)除(chu)箱(xiang)體(ti)內(nei)的(de)水(shui),做(zuo)好(hao)儀(yi)器(qi)使(shi)用(yong)記(ji)錄(lu)。燒杯因其口徑上下一致,是取用液體、配製溶液、做簡單化學反應最常用的反應容器。但燒杯不能代替量筒量取液體。燒杯加熱時要墊上石棉網。不能用火焰直接加熱燒杯。因為燒杯底麵大,用火焰直接加熱,隻可燒到局部,使玻璃受熱不勻而引起炸裂。用燒杯加熱液體時,液體的量以不超過燒杯容積的1/3為(wei)宜(yi),以(yi)防(fang)沸(fei)騰(teng)時(shi)液(ye)體(ti)外(wai)溢(yi)。加(jia)熱(re)時(shi),燒(shao)杯(bei)外(wai)壁(bi)須(xu)擦(ca)幹(gan)。加(jia)熱(re)腐(fu)蝕(shi)性(xing)藥(yao)品(pin)時(shi),可(ke)將(jiang)一(yi)表(biao)麵(mian)皿(min)蓋(gai)在(zai)燒(shao)杯(bei)口(kou)上(shang),以(yi)免(mian)液(ye)體(ti)濺(jian)出(chu)。不(bu)可(ke)用(yong)燒(shao)杯(bei)長(chang)期(qi)盛(sheng)放(fang)化(hua)學(xue)藥(yao)品(pin),以(yi)免(mian)落(luo)入(ru)塵(chen)土(tu)和(he)使(shi)溶(rong)液(ye)中(zhong)的(de)水(shui)分(fen)蒸(zheng)發(fa)。溶(rong)解(jie)或(huo)稀(xi)釋(shi)過(guo)程(cheng)中(zhong),用(yong)玻(bo)璃(li)棒(bang)攪(jiao)拌(ban)時(shi),不(bu)要(yao)觸(chu)及(ji)杯(bei)底(di)或(huo)杯(bei)壁(bi)。實驗室用來盛放少量藥品,加熱情況下少量試劑反應的容器。裝溶液時不超過試管容量的1/2,加熱時不超過試管的1/3。取塊狀固體放入試管要用鑷子,不能使固體直接墜入試管中,防止試管底破裂。加熱時使用試管夾,試管夾應夾在距管口1/3處。試管口不能對著人。試管不可以直接加熱,要先預熱,加熱盛有固體的試管時,管口略向下,加熱液體時傾斜約45°。加(jia)熱(re)時(shi)要(yao)保(bao)持(chi)試(shi)管(guan)外(wai)壁(bi)沒(mei)有(you)水(shui)珠(zhu),防(fang)止(zhi)受(shou)熱(re)不(bu)均(jun)勻(yun)而(er)爆(bao)裂(lie)。加(jia)熱(re)後(hou)不(bu)能(neng)驟(zhou)冷(leng),防(fang)止(zhi)試(shi)管(guan)破(po)裂(lie)。加(jia)熱(re)後(hou)不(bu)能(neng)在(zai)試(shi)管(guan)未(wei)冷(leng)卻(que)至(zhi)室(shi)溫(wen)時(shi)就(jiu)洗(xi)滌(di)試(shi)管(guan)。加(jia)熱(re)時(shi)應(ying)用(yong)外(wai)焰(yan)。容(rong)量(liang)瓶(ping)主(zhu)要(yao)用(yong)於(yu)準(zhun)確(que)地(di)配(pei)製(zhi)一(yi)定(ding)摩(mo)爾(er)濃(nong)度(du)的(de)溶(rong)液(ye),它(ta)是(shi)一(yi)種(zhong)細(xi)長(chang)頸(jing),梨(li)形(xing)的(de)平(ping)底(di)玻(bo)璃(li)瓶(ping),帶(dai)有(you)磨(mo)口(kou)玻(bo)璃(li)塞(sai),瓶(ping)頸(jing)上(shang)刻(ke)有(you)標(biao)線(xian),當(dang)瓶(ping)內(nei)液(ye)體(ti)在(zai)所(suo)指(zhi)定(ding)溫(wen)度(du)下(xia)達(da)到(dao)標(biao)線(xian)處(chu)時(shi),其(qi)體(ti)積(ji)即(ji)為(wei)瓶(ping)上(shang)所(suo)注(zhu)明(ming)的(de)容(rong)積(ji)數(shu)。容(rong)量(liang)瓶(ping)不(bu)能(neng)配(pei)製(zhi)其(qi)容(rong)積(ji)以(yi)下(xia)體(ti)積(ji)的(de)溶(rong)液(ye),即(ji)其(qi)容(rong)積(ji)為(wei)多(duo)大(da),就(jiu)隻(zhi)能(neng)配(pei)製(zhi)多(duo)大(da)體(ti)積(ji)的(de)溶(rong)液(ye)。容(rong)量(liang)瓶(ping)使(shi)用(yong)前(qian)應(ying)先(xian)檢(jian)查(zha)是(shi)否(fou)漏(lou)水(shui),依(yi)次(ci)用(yong)自(zi)來(lai)水(shui),蒸(zheng)餾(liu)水(shui)洗(xi)好(hao)備(bei)用(yong)。將(jiang)溶(rong)質(zhi)在(zai)燒(shao)杯(bei)中(zhong)溶(rong)解(jie)後(hou)轉(zhuan)移(yi)到(dao)容(rong)量(liang)瓶(ping)裏(li),不(bu)能(neng)在(zai)容(rong)量(liang)瓶(ping)裏(li)進(jin)行(xing)溶(rong)質(zhi)的(de)溶(rong)解(jie),控(kong)製(zhi)溶(rong)解(jie)溶(rong)質(zhi)的(de)蒸(zheng)餾(liu)水(shui)量(liang)。zhuanyishibixuyongbolibangyinliu。rongliangpingbunengjinxingjiare,ruguorongzhizairongjieguochengzhongfangre,yaodairongyelengquehouzaijinxingzhuanyi,yinweiwendushenggaopingtijiangpengzhang,suoliangtijijiuhuibuzhunque。yongyuxidishaobeiderongjizongliangbunengchaoguorongliangpingdebiaoxian,yidanchaoguo,bixuzhongxinjinxingpeizhi。peizhihaoderongyezhuanyizhishijipingzhongbaocun,rongliangpingzhinengpeizhirongye,bunengchucunrongye,yinweirongyekenenghuiduipingtijinxingfushi,congershirongliangpingdejingdushoudaoyingxiang。rongliangpingshiyongwanbiyingjishiyongshuichongxiganjing,saishangpingsai,bingzaisaiziyupingkouzhijianjiayitiaozhitiao,fangzhipingsaiyupingkouzhanlian。zuihoujilurongyetijideshihouyibanbaoliu4位有效數字(XXX.0mL)。滴定管是可放出不固定量液體的量出式玻璃儀器,主要用於滴定分析中對滴定劑體積的測量。能精確到到0.01mL。帶玻璃活塞的滴定管為酸式滴定管,帶有內裝玻璃球的橡皮管的滴定管為堿式滴定管。酸式、堿式滴定管不能混用,酸式滴定管裝酸性物質和大多數中性物質(尤其是強氧化劑),堿式滴定管裝堿性物質(包括堿和堿性鹽),滴定管使用前先檢查是否漏液,如果漏水,應重新將活塞塗凡士林油。裝液前要用洗液、水依次衝洗幹淨,並要用待裝的溶液潤洗滴定管。將jiang操cao作zuo溶rong液ye倒dao入ru,直zhi到dao充chong滿man至zhi零ling刻ke度du線xian以yi上shang為wei止zhi。注zhu意yi檢jian查zha滴di定ding管guan的de出chu口kou管guan是shi否fou充chong滿man溶rong液ye,如ru有you氣qi泡pao進jin行xing排pai氣qi泡pao操cao作zuo。調tiao整zheng液ye麵mian時shi,使shi液ye麵mian保bao持chi在zai“0”或“0”以yi下xia的de某mou一yi定ding刻ke度du。進jin行xing滴di定ding時shi,應ying將jiang滴di定ding管guan垂chui直zhi地di夾jia在zai滴di定ding管guan夾jia上shang,如ru使shi用yong的de是shi堿jian式shi滴di定ding管guan,拇mu指zhi與yu食shi指zhi在zai玻bo璃li珠zhu所suo在zai部bu位wei一yi旁pang捏nie乳ru膠jiao管guan,不bu要yao捏nie玻bo璃li珠zhu,也ye不bu能neng使shi其qi上shang下xia移yi動dong。滴di定ding時shi應ying逐zhu滴di連lian續xu滴di加jia,接jie近jin終zhong點dian時shi,隻zhi加jia一yi滴di或huo半ban滴di,至zhi溶rong液ye出chu現xian明ming顯xian的de顏yan色se變bian化hua。讀數時,手拿滴定管上部無刻度處,使滴定管保持垂直,視線平視溶液的凹液麵,讀到小數點後第二位,即估計到0.01mL。滴定結束後,管內剩餘的溶液應棄去,不得將其倒回原瓶,隨即清洗滴定管,並倒掛於鐵架台上。 實驗室常用的玻璃儀器如燒杯、試管、滴定管、移液管、容量瓶等。儀器在使用中會沾上油汙,水垢,鏽跡等,使用後不及時完全的清洗,會造成結果誤差,甚至會對儀器的壽命、性能會產生極其不良的影響。因此,化學實驗使用的玻璃儀器必須洗滌幹淨。下麵介紹一些玻璃儀器的洗滌方法。fuyouyiquchuwuzhidejiandanyiqi,rushiguan。shaobeideng,xianyongzilaishuichongxi,zaiyongshiguanshuazhanquhechengxidijishuaxi,zuihouzilaishuichongxi。dangdaozhiyiqi,qibixingchengyicengjunyundeshuimo,buchengguliuxiashi,jiyixijing。youyouwudeboliqimin,xianyongjianxingjiujingxidiyexidi,ranhouyongxiyifenshuihuofeizaoshuixidi,zaiyongzilaishuichongxiganjing。youxiuji,shuigoudeqimin,yong(1+3)鹽yan酸suan洗xi液ye浸jin泡pao,再zai用yong再zai來lai水shui衝chong洗xi幹gan淨jing。有you凡fan士shi林lin油you汙wu的de器qi皿min,先xian將jiang凡fan士shi林lin擦ca去qu,再zai用yong洗xi衣yi粉fen水shui或huo肥fei皂zao水shui洗xi燒shao煮zhu,取qu出chu後hou用yong自zi來lai水shui衝chong洗xi幹gan淨jing。一yi些xie構gou造zao比bi較jiao精jing細xi、複雜的玻璃儀器,如容量瓶、移液管等,無法用毛刷刷洗,可以用洗滌液浸泡一定時間,再進行清洗。洗淨的玻璃儀器不要再用手、布或紙擦拭,以免重新汙染。實驗室常用的光學儀器如分光光度計、折光計的棱鏡、玻片等,都是一些精密光學儀器,在使用和保養中,必須細心謹慎,嚴格按說明使用,不得任意鬆動儀器各連接部分,不得跌落、碰撞儀器,以防止光學零件損傷及影響精度。
被bei測ce試shi樣yang中zhong不bu應ying有you硬ying性xing雜za質zhi,當dang測ce試shi固gu體ti試shi樣yang時shi,應ying防fang止zhi把ba折zhe射she棱leng鏡jing表biao麵mian拉la毛mao或huo產chan生sheng壓ya痕hen。使shi用yong完wan畢bi後hou,嚴yan禁jin直zhi接jie放fang入ru水shui中zhong清qing洗xi,避bi免mian光guang學xue係xi統tong管guan路lu進jin水shui。打da開kai棱leng鏡jing,用yong擦ca鏡jing紙zhi輕qing輕qing擦ca幹gan,不bu論lun在zai任ren何he情qing況kuang下xia,不bu允yun許xu用yong擦ca鏡jing紙zhi以yi外wai的de任ren何he東dong西xi接jie觸chu到dao棱leng鏡jing,以yi免mian損sun壞huai它ta的de光guang學xue平ping麵mian。儀yi器qi應ying存cun放fang於yu幹gan燥zao、無灰塵、無油汙和無有害、易燃、易爆等氣體的地方,以免光學零件腐蝕或生黴。光學儀器在使用中容易沾上油汙、水濕性汙物、指紋等,影響成像及透光率。清洗折光計的棱鏡、平麵鏡、顯xian微wei鏡jing的de鏡jing頭tou,先xian用yong蒸zheng餾liu水shui進jin行xing清qing洗xi,鏡jing麵mian若ruo有you汙wu漬zi,可ke以yi用yong乙yi醇chun和he乙yi醚mi的de混hun合he液ye清qing洗xi。清qing洗xi時shi用yong專zhuan門men的de擦ca鏡jing紙zhi或huo棉mian球qiu沾zhan有you少shao量liang清qing洗xi劑ji,順shun著zhe一yi個ge方fang向xiang擦ca拭shi,從cong鏡jing頭tou中zhong心xin向xiang外wai作zuo圓yuan運yun動dong,切qie忌ji把ba這zhe類lei鏡jing頭tou浸jin泡pao在zai清qing洗xi劑ji中zhong清qing洗xi。清qing洗xi鏡jing頭tou不bu得de用yong力li拭shi擦ca,否fou則ze會hui劃hua傷shang增zeng透tou膜mo,損sun壞huai鏡jing頭tou。清qing洗xi完wan畢bi後hou用yong擦ca鏡jing紙zhi擦ca幹gan,避bi光guang保bao存cun。