有的用戶如果對微量元素分析儀的專業知識缺乏或了解甚少,不要擔心,隻要掌握以下幾個要點,便可輕鬆應對。
diyishizhongfuxingwendingxing,zheshiyiqizuijibendeyaoqiu,shifenxijianyandejichu。zhexiangzhibiaobuhao,qitajiuwucongtanqi,chuncuishihuyoule。ruguotongyigeyangpin,jiancehuodejieguohugaohudi,xiangchahenda,zheshuomingyiqiyouwenti。ruguonikanyiqishice,yixiechangjiaweibimianfangbiandiguancezhongfuxing,burangcaozuozhenengfangbiandidiejiaquxian,bushezhiqiubianyixishudechengxu,zhejiushiyinweiyiqidexingnengbujia,pabeibierenyiyankanchuwenti,shengchanshangzaihuibizhegewenti。shijishangyixiechangjiadeyiqibianyixishuzai10—20%之間,誤差大大超過了有關規定,這樣做出的結果可信度低,我公司產品的變異係數內控在5%以下,通過儀器的測試可一目了然。
電化學中極譜分析使用的電極極小(指滴汞電),而靈敏度與電極比表麵積有關,麵積大信噪比高(指信號與噪聲的比值),靈(ling)敏(min)度(du)高(gao),抗(kang)幹(gan)擾(rao)能(neng)力(li)強(qiang),但(dan)由(you)於(yu)滴(di)汞(gong)電(dian)極(ji)麵(mian)積(ji)取(qu)決(jue)於(yu)體(ti)積(ji),大(da)了(le)就(jiu)要(yao)不(bu)受(shou)控(kong)的(de)脫(tuo)落(luo),因(yin)此(ci)電(dian)極(ji)表(biao)麵(mian)積(ji)受(shou)到(dao)嚴(yan)重(zhong)製(zhi)約(yue),這(zhe)決(jue)定(ding)了(le)常(chang)規(gui)方(fang)式(shi)電(dian)極(ji)所(suo)做(zuo)的(de)儀(yi)器(qi)噪(zao)聲(sheng)大(da),重(zhong)複(fu)性(xing)不(bu)佳(jia),這(zhe)是(shi)目(mu)前(qian)所(suo)有(you)使(shi)用(yong)這(zhe)類(lei)電(dian)極(ji)儀(yi)器(qi)一(yi)個(ge)通(tong)病(bing)。隻(zhi)有(you)我(wo)公(gong)司(si)的(de)產(chan)品(pin)通(tong)過(guo)采(cai)用(yong)靜(jing)汞(gong)電(dian)極(ji)等(deng)一(yi)係(xi)列(lie)技(ji)術(shu)解(jie)決(jue)好(hao)這(zhe)個(ge)問(wen)題(ti)。在(zai)這(zhe)個(ge)技(ji)術(shu)領(ling)域(yu)是(shi)勝(sheng)過(guo)任(ren)何(he)一(yi)款(kuan)同(tong)類(lei)儀(yi)器(qi),這(zhe)可(ke)通(tong)過(guo)現(xian)場(chang)比(bi)較(jiao)來(lai)證(zheng)實(shi)。另(ling)外(wai)一(yi)類(lei)電(dian)化(hua)學(xue)儀(yi)器(qi)則(ze)回(hui)避(bi)了(le)這(zhe)類(lei)問(wen)題(ti),采(cai)用(yong)固(gu)體(ti)電(dian)極(ji)來(lai)測(ce)所(suo)有(you)元(yuan)素(su),並(bing)從(cong)環(huan)保(bao)角(jiao)度(du)攻(gong)擊(ji)使(shi)用(yong)極(ji)譜(pu)方(fang)法(fa)的(de)儀(yi)器(qi)使(shi)用(yong)了(le)汞(gong)電(dian)極(ji)。其(qi)實(shi)在(zai)檢(jian)測(ce)中(zhong),汞(gong)都(dou)在(zai)封(feng)閉(bi)環(huan)境(jing)中(zhong)工(gong)作(zuo),不(bu)與(yu)大(da)氣(qi)接(jie)觸(chu)。就(jiu)如(ru)血(xue)壓(ya)計(ji),目(mu)前(qian)的(de)測(ce)的(de)準(zhun)的(de)還(hai)是(shi)水(shui)銀(yin)血(xue)壓(ya)計(ji),還(hai)在(zai)廣(guang)泛(fan)使(shi)用(yong)。使(shi)用(yong)滴(di)汞(gong)電(dian)極(ji)的(de)極(ji)譜(pu)分(fen)析(xi)方(fang)法(fa),在(zai)很(hen)多(duo)領(ling)域(yu)裏(li)都(dou)是(shi)國(guo)標(biao)法(fa)和(he)行(xing)業(ye)標(biao)準(zhun)。例(li)如(ru)血(xue)清(qing)中(zhong)鋅(xin)測(ce)定(ding)是(shi)衛(wei)生(sheng)部(bu)檢(jian)驗(yan)規(gui)程(cheng)規(gui)定(ding)方(fang)法(fa),而(er)食(shi)品(pin)中(zhong)極(ji)譜(pu)分(fen)析(xi)標(biao)準(zhun)更(geng)多(duo)。而(er)使(shi)用(yong)固(gu)體(ti)電(dian)極(ji)(如玻碳電極)測ce某mou些xie特te定ding元yuan素su如ru鉛qian效xiao果guo是shi好hao的de,但dan以yi不bu變bian應ying萬wan變bian用yong其qi來lai解jie決jue所suo有you元yuan素su的de檢jian測ce是shi不bu可ke能neng的de,無wu論lun是shi從cong理li論lun上shang還hai是shi實shi踐jian上shang都dou缺que少shao佐zuo證zheng。那na些xie花hua大da價jia錢qian買mai這zhe類lei儀yi器qi的de,要yao麼me就jiu是shi知zhi識shi不bu夠gou,要yao麼me是shi另ling有you原yuan因yin。微wei量liang元yuan素su分fen析xi因yin含han量liang低di,有you用yong信xin號hao小xiao,對dui技ji術shu要yao求qiu很hen高gao。做zuo的de好hao的de重zhong複fu性xing好hao,靈ling敏min度du高gao,儀yi器qi性xing能neng穩wen定ding,做zuo不bu好hao的de,重zhong複fu性xing差cha,整zheng個ge儀yi器qi基ji礎chu差cha,就jiu要yao用yong各ge種zhong手shou段duan應ying付fu用yong戶hu,隱yin瞞man真zhen相xiang,而er用yong戶hu對dui此ci知zhi之zhi甚shen少shao。最zui簡jian單dan判pan斷duan方fang法fa是shi看kan儀yi器qi是shi否fou設she置zhi了le能neng方fang便bian地di進jin行xing多duo條tiao曲qu線xian迭die加jia比bi較jiao、直zhi接jie觀guan察cha重zhong複fu性xing功gong能neng,能neng否fou方fang便bian地di求qiu變bian異yi係xi數shu。再zai進jin一yi步bu實shi測ce一yi下xia血xue中zhong鋅xin,多duo次ci檢jian測ce看kan重zhong複fu性xing好hao壞huai,因yin鋅xin的de含han量liang較jiao低di,能neng考kao核he儀yi器qi的de性xing能neng,做zuo之zhi前qian需xu檢jian測ce一yi下xia空kong白bai,防fang止zhi試shi劑ji空kong白bai過guo高gao造zao成cheng假jia象xiang。
在zai做zuo好hao重zhong複fu性xing的de基ji礎chu上shang才cai有you可ke能neng考kao察cha其qi他ta性xing能neng指zhi標biao,客ke觀guan的de說shuo,隻zhi要yao重zhong複fu性xing做zuo好hao了le,其qi他ta性xing能neng指zhi標biao應ying問wen題ti不bu大da。但dan是shi那na種zhong用yong一yi種zhong電dian極ji做zuo所suo有you元yuan素su的de儀yi器qi,做zuo空kong白bai加jia標biao準zhun溶rong液ye和he實shi測ce樣yang品pin有you天tian壤rang之zhi別bie。就jiu是shi說shuo如ru果guo不bu做zuo樣yang品pin隻zhi做zuo單dan純chun的de標biao準zhun溶rong液ye,可ke能neng很hen好hao,但dan是shi加jia入ru樣yang品pin,樣yang品pin帶dai來lai各ge種zhong幹gan擾rao使shi重zhong複fu性xing、線性、靈敏度都有非常大的變化。目前使用固體玻炭電極測血鉛比較成熟。其他應看看國家、行(xing)業(ye)有(you)無(wu)這(zhe)方(fang)麵(mian)的(de)標(biao)準(zhun),有(you)沒(mei)有(you)這(zhe)方(fang)麵(mian)的(de)文(wen)獻(xian),有(you)文(wen)獻(xian)的(de)有(you)沒(mei)有(you)實(shi)際(ji)用(yong)於(yu)樣(yang)品(pin)的(de)範(fan)例(li)。如(ru)果(guo)都(dou)沒(mei)有(you),有(you)的(de)企(qi)業(ye)卻(que)在(zai)很(hen)短(duan)的(de)時(shi)間(jian)內(nei)用(yong)這(zhe)種(zhong)電(dian)極(ji)搞(gao)出(chu)了(le)一(yi)套(tao)分(fen)析(xi)方(fang)法(fa),究(jiu)竟(jing)是(shi)能(neng)力(li)超(chao)強(qiang)還(hai)是(shi)另(ling)有(you)原(yuan)因(yin),就(jiu)需(xu)感(gan)興(xing)趣(qu)者(zhe)自(zi)己(ji)考(kao)慮(lv)了(le)。
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