與薄膜的力學、熱(re)學(xue)性(xing)能(neng)檢(jian)測(ce)相(xiang)比(bi),阻(zu)隔(ge)性(xing)檢(jian)測(ce)的(de)對(dui)象(xiang)更(geng)加(jia)微(wei)觀(guan),測(ce)試(shi)原(yuan)理(li)更(geng)加(jia)複(fu)雜(za),而(er)且(qie)阻(zu)隔(ge)性(xing)檢(jian)測(ce)設(she)備(bei)與(yu)常(chang)規(gui)項(xiang)目(mu)的(de)檢(jian)測(ce)設(she)備(bei)相(xiang)比(bi)要(yao)昂(ang)貴(gui)地(di)多(duo),因(yin)此(ci)對(dui)設(she)備(bei)進(jin)行(xing)維(wei)護(hu)以(yi)盡(jin)可(ke)能(neng)地(di)延(yan)長(chang)其(qi)使(shi)用(yong)時(shi)間(jian)進(jin)而(er)提(ti)高(gao)設(she)備(bei)的(de)利(li)用(yong)率(lv)是(shi)很(hen)有(you)必(bi)要(yao)的(de)。此(ci)外(wai),盡(jin)管(guan)早(zao)期(qi)阻(zu)隔(ge)性(xing)測(ce)試(shi)中(zhong)有(you)很(hen)多(duo)步(bu)驟(zhou)需(xu)要(yao)人(ren)工(gong)操(cao)作(zuo),當(dang)前(qian)的(de)設(she)備(bei)自(zi)動(dong)化(hua)程(cheng)度(du)卻(que)已(yi)經(jing)相(xiang)當(dang)高(gao)了(le),基(ji)本(ben)上(shang)除(chu)去(qu)試(shi)樣(yang)裝(zhuang)夾(jia)步(bu)驟(zhou),設(she)備(bei)可(ke)自(zi)動(dong)完(wan)成(cheng)整(zheng)個(ge)試(shi)驗(yan)直(zhi)到(dao)出(chu)具(ju)檢(jian)測(ce)數(shu)據(ju),因(yin)此(ci)檢(jian)測(ce)設(she)備(bei)工(gong)作(zuo)狀(zhuang)態(tai)的(de)好(hao)壞(huai)可(ke)以(yi)說(shuo)是(shi)決(jue)定(ding)測(ce)試(shi)數(shu)據(ju)準(zhun)確(que)性(xing)的(de)首(shou)要(yao)因(yin)素(su)。可(ke)見(jian),如(ru)何(he)合(he)理(li)地(di)維(wei)護(hu)阻(zu)隔(ge)性(xing)設(she)備(bei)、讓rang設she備bei長chang時shi間jian地di保bao持chi穩wen定ding正zheng常chang的de工gong作zuo狀zhuang態tai是shi非fei常chang重zhong要yao的de。由you於yu檢jian測ce原yuan理li以yi及ji關guan鍵jian元yuan器qi件jian的de不bu同tong,各ge類lei阻zu隔ge性xing檢jian測ce設she備bei的de維wei護hu方fang法fa存cun在zai很hen大da差cha異yi,本ben文wen將jiang按an照zhao測ce試shi方fang法fa對dui設she備bei的de維wei護hu重zhong點dian進jin行xing介jie紹shao。
1. 透氣性測試設備
1.1 壓差法
yachafajuyouhenduoyoudian,qizhongzuizhuyaodeyigeyoudianshitaduiyuceshiqitimeiyouxuanzexing,erqiechuanganqiyebingfeisunhaoxing,bucunzaishiyongshijianheshiyongliangdexianzhi。yinciduiyuyachafashebeilaijiang,zhuyicaozuoxijieshijinxingshebeiweihudezhongdian。shouxian,bimianyouyiwujinruceshixiaqiang,youyuceshixiaqiangyuzhenkongbengshizhijiexiangliande,suoyiruguoxiaqiangzhongcunzaiyiwuzehuibeichouruzhenkongbengnei,duizhenkongbengzaochengsunhuai。qici,zhenkongbengyouyingshiyongchangjiatigongdezhenkongbengzhuanyongyou,zaishiyongshizhenkongbengneideyouliangyingkongzhizaiguidingdefanweinei,bingzhuyiyouzhidebianhua。disan,duiyuzaoqideyachafashebei,youxiezhenkongceyajishihanyoushuiyinchengfendezhuangzhi,zheshixuyaotebiezhuyishuiyindecunfanganquan。
1.2 等壓法
dengyafashebeizhuyaocaiyongyangchuanganqijinxingcailiaodetouyangxingjiance,ercaiyongdeyangchuanganqishisunhaoxingde,qizhongdeyouxiaotancechengfenhuisuizheceshishijiandeyanchangerzhubusunhao,erjiangqibaoluzaigaonongdudeyangqihuokongqizhonghuihenkuaibeixiaohaoerwufazaijixushiyong。genghuanyangchuanganqichengbenanggui,yinciweihudengyafashebeizuizhongyaodeyidianshibaohuyangchuanganqigejuewaijieqitiyiyanchangqishiyongshouming。shouxianyaoquebaoshiyangzhuangjiawanhao,bimianxielou。qicizaishiyanguochengzhongyaoxianduiceshixitongjinxingchuisao,zhidaoqizhongdeyanghanliangjiangdaojididezhuangtaihouzaijinrushentouguocheng,tongshiruoshiyangdetouyangliangjiaodayexuyaocaiqucuoshifangzhiyangchuanganqineideyanghanliangchixupiangaoyijianshaoyangchuanganqidesunhao。Labthink係(xi)列(lie)等(deng)壓(ya)法(fa)設(she)備(bei)提(ti)供(gong)利(li)用(yong)輔(fu)助(zhu)工(gong)具(ju)減(jian)小(xiao)試(shi)樣(yang)的(de)測(ce)試(shi)麵(mian)積(ji)以(yi)及(ji)增(zeng)加(jia)載(zai)氣(qi)流(liu)速(su)兩(liang)種(zhong)方(fang)法(fa)來(lai)降(jiang)低(di)氧(yang)傳(chuan)感(gan)器(qi)的(de)損(sun)耗(hao),實(shi)際(ji)檢(jian)測(ce)證(zheng)明(ming)這(zhe)兩(liang)種(zhong)方(fang)法(fa)不(bu)但(dan)可(ke)以(yi)降(jiang)低(di)氧(yang)傳(chuan)感(gan)器(qi)有(you)效(xiao)探(tan)測(ce)物(wu)質(zhi)在(zai)檢(jian)測(ce)過(guo)程(cheng)中(zhong)的(de)損(sun)耗(hao),而(er)且(qie)還(hai)可(ke)以(yi)大(da)大(da)擴(kuo)展(zhan)設(she)備(bei)的(de)測(ce)試(shi)量(liang)程(cheng)。再(zai)次(ci),在(zai)試(shi)驗(yan)結(jie)束(shu)後(hou)必(bi)須(xu)將(jiang)氧(yang)傳(chuan)感(gan)器(qi)內(nei)氣(qi)體(ti)的(de)氧(yang)含(han)量(liang)降(jiang)到(dao)最(zui)低(di),若(ruo)儀(yi)器(qi)近(jin)期(qi)還(hai)要(yao)做(zuo)試(shi)驗(yan),可(ke)先(xian)用(yong)大(da)流(liu)量(liang)載(zai)氣(qi)對(dui)測(ce)試(shi)腔(qiang)進(jin)行(xing)吹(chui)掃(sao)然(ran)後(hou)再(zai)把(ba)載(zai)氣(qi)流(liu)速(su)調(tiao)小(xiao)並(bing)持(chi)續(xu)吹(chui)掃(sao)係(xi)統(tong)以(yi)防(fang)止(zhi)外(wai)界(jie)氧(yang)氣(qi)的(de)滲(shen)入(ru);若近期不使用設備隻有在確認氣流的氧含量足夠少時(如係統被高純氮氣吹掃2小時以上),才可關閉氧傳感器保護閥然後關閉鋼瓶輸出閥停止供氣。Labthink係xi列lie等deng壓ya法fa設she備bei設she置zhi了le雙shuang重zhong氧yang傳chuan感gan器qi保bao護hu措cuo施shi,大da大da改gai良liang了le密mi封feng效xiao果guo。然ran而er由you於yu傳chuan感gan器qi的de損sun耗hao直zhi接jie影ying響xiang測ce試shi數shu據ju的de準zhun確que性xing,所suo以yi等deng壓ya法fa設she備bei必bi須xu定ding期qi標biao定ding。
還(hai)需(xu)特(te)別(bie)注(zhu)意(yi)的(de)一(yi)點(dian)是(shi),等(deng)壓(ya)法(fa)設(she)備(bei)無(wu)論(lun)是(shi)在(zai)測(ce)試(shi)過(guo)程(cheng)中(zhong)還(hai)是(shi)在(zai)試(shi)驗(yan)結(jie)束(shu)之(zhi)後(hou)總(zong)需(xu)要(yao)用(yong)大(da)量(liang)載(zai)氣(qi)吹(chui)掃(sao)測(ce)試(shi)係(xi)統(tong),因(yin)此(ci)試(shi)驗(yan)尾(wei)氣(qi)排(pai)放(fang)量(liang)相(xiang)當(dang)大(da),所(suo)以(yi)必(bi)須(xu)注(zhu)意(yi)對(dui)尾(wei)氣(qi)的(de)處(chu)理(li)。應(ying)該(gai)使(shi)用(yong)導(dao)氣(qi)管(guan)連(lian)接(jie)儀(yi)器(qi)的(de)尾(wei)氣(qi)出(chu)氣(qi)口(kou)並(bing)將(jiang)尾(wei)氣(qi)引(yin)到(dao)室(shi)外(wai),同(tong)時(shi)應(ying)注(zhu)意(yi)室(shi)內(nei)的(de)空(kong)氣(qi)循(xun)環(huan),保(bao)持(chi)空(kong)氣(qi)清(qing)新(xin)。
disan,xianzaidedengyafashebeipubianjuyouduiceshiqitiwenshidudekongzhigongneng,duiceshiqitikongshibukebimiandiyaozaiqiluzhongzengjiashidufashengwuzhi,erzaiqiluzhongchangshijiancunyoushiqibuliyushebeiweihu,yincizaijiashishiyanjieshuzhihouxuyaojiangshiduzengjiazhuangzhizhongdeshidufashengwuzhiqingchuganjingbingyongganzaodanqichuijingxitongzhongdeshiqi。
2. 透濕性測試設備
2.1 稱重法
chengzhongfashitoushixingceshidejichuceshifangfa,zishangshijizhongyejiuyijingkaishishiyong,yincizaiyingyonglingyuzhongshijishiyongdegaileishebeizidonghuachengduchayijiaoda,zaoqifeizidongjianceshebeiyudangqiandezidongjianceshebeizaiweihufangfashangyeyousuobutong。duiyuzaoqifeizidongjianceshebei,xuyaocaiyonghengwenhengshixiang、透濕杯、稱重天平等分離物件進行組合測試,因此對它們的維護也是分離進行的,控製的重點在於保證透濕杯和稱重天平表麵清潔、無(wu)腐(fu)蝕(shi)。而(er)對(dui)於(yu)現(xian)在(zai)廣(guang)泛(fan)使(shi)用(yong)的(de)自(zi)動(dong)檢(jian)測(ce)設(she)備(bei),在(zai)試(shi)驗(yan)結(jie)束(shu)之(zhi)後(hou)需(xu)將(jiang)透(tou)濕(shi)杯(bei)從(cong)設(she)備(bei)中(zhong)取(qu)出(chu),清(qing)理(li)透(tou)濕(shi)杯(bei)內(nei)部(bu),保(bao)持(chi)幹(gan)燥(zao)潔(jie)淨(jing)的(de)狀(zhuang)態(tai)即(ji)可(ke)。同(tong)時(shi),為(wei)防(fang)止(zhi)設(she)備(bei)中(zhong)元(yuan)器(qi)件(jian)鏽(xiu)蝕(shi),加(jia)濕(shi)物(wu)質(zhi)必(bi)須(xu)使(shi)用(yong)指(zhi)定(ding)的(de)蒸(zheng)餾(liu)水(shui)或(huo)者(zhe)試(shi)劑(ji)。
2.2 傳感器法
對(dui)於(yu)紅(hong)外(wai)傳(chuan)感(gan)器(qi)法(fa)以(yi)及(ji)電(dian)解(jie)傳(chuan)感(gan)器(qi)法(fa)來(lai)講(jiang),它(ta)們(men)采(cai)用(yong)的(de)水(shui)蒸(zheng)氣(qi)傳(chuan)感(gan)器(qi)是(shi)消(xiao)耗(hao)型(xing)的(de),有(you)效(xiao)測(ce)試(shi)成(cheng)分(fen)會(hui)隨(sui)著(zhe)測(ce)試(shi)時(shi)間(jian)的(de)延(yan)長(chang)而(er)逐(zhu)漸(jian)消(xiao)耗(hao),水(shui)蒸(zheng)氣(qi)傳(chuan)感(gan)器(qi)使(shi)用(yong)成(cheng)本(ben)較(jiao)高(gao),因(yin)此(ci)設(she)備(bei)的(de)維(wei)護(hu)重(zhong)點(dian)是(shi)水(shui)蒸(zheng)氣(qi)傳(chuan)感(gan)器(qi)。在(zai)試(shi)驗(yan)過(guo)程(cheng)中(zhong)應(ying)盡(jin)量(liang)降(jiang)低(di)試(shi)樣(yang)透(tou)過(guo)的(de)水(shui)蒸(zheng)氣(qi)量(liang),例(li)如(ru)減(jian)小(xiao)試(shi)樣(yang)的(de)測(ce)試(shi)麵(mian)積(ji)。在(zai)試(shi)驗(yan)結(jie)束(shu)後(hou),若(ruo)近(jin)期(qi)需(xu)要(yao)進(jin)行(xing)試(shi)驗(yan),可(ke)持(chi)續(xu)用(yong)大(da)流(liu)量(liang)的(de)幹(gan)燥(zao)高(gao)純(chun)氮(dan)氣(qi)吹(chui)洗(xi)管(guan)路(lu)直(zhi)到(dao)下(xia)次(ci)試(shi)驗(yan);若ruo近jin期qi不bu需xu使shi用yong儀yi器qi,需xu要yao先xian將jiang測ce試shi濕shi腔qiang中zhong的de加jia濕shi物wu質zhi取qu出chu,並bing用yong幹gan燥zao濾lv紙zhi把ba附fu著zhe在zai腔qiang壁bi上shang的de水shui吸xi幹gan,再zai將jiang鋁lv箔bo複fu合he膜mo裝zhuang夾jia在zai試shi驗yan腔qiang中zhong,並bing以yi幹gan燥zao高gao純chun氮dan氣qi持chi續xu吹chui掃sao測ce試shi腔qiang若ruo幹gan小xiao時shi,然ran後hou關guan閉bi傳chuan感gan器qi保bao護hu閥fa封feng閉bi水shui蒸zheng氣qi傳chuan感gan器qi,最zui後hou關guan閉bi鋼gang瓶ping輸shu出chu閥fa。隻zhi有you水shui蒸zheng氣qi傳chuan感gan器qi保bao持chi穩wen定ding正zheng常chang的de工gong作zuo狀zhuang態tai,設she備bei才cai能neng出chu具ju正zheng確que的de試shi驗yan結jie果guo,因yin此ci需xu要yao對dui傳chuan感gan器qi法fa設she備bei進jin行xing定ding期qi標biao定ding,以yi確que保bao測ce試shi數shu據ju的de準zhun確que性xing。其qi次ci,要yao注zhu意yi在zai試shi驗yan結jie束shu之zhi後hou對dui測ce試shi係xi統tong中zhong的de濕shi氣qi進jin行xing處chu理li,保bao證zheng其qi內nei部bu幹gan燥zao,尤you其qi是shi當dang近jin期qi不bu需xu要yao使shi用yong設she備bei的de時shi候hou。第di三san,這zhe兩liang種zhong方fang法fa無wu論lun是shi在zai測ce試shi過guo程cheng中zhong還hai是shi在zai試shi驗yan結jie束shu之zhi後hou總zong需xu要yao用yong大da量liang載zai氣qi吹chui掃sao測ce試shi係xi統tong,因yin此ci試shi驗yan尾wei氣qi排pai放fang量liang相xiang當dang大da,所suo以yi必bi須xu注zhu意yi對dui尾wei氣qi的de處chu理li。試shi驗yan尾wei氣qi應ying通tong過guo導dao氣qi管guan排pai到dao室shi外wai,同tong時shi注zhu意yi室shi內nei通tong風feng。第di四si,為wei避bi免mian設she備bei中zhong元yuan器qi件jian鏽xiu蝕shi,加jia濕shi物wu質zhi必bi須xu使shi用yong指zhi定ding的de蒸zheng餾liu水shui或huo者zhe試shi劑ji。
對dui於yu濕shi度du傳chuan感gan器qi法fa,由you於yu所suo采cai用yong的de傳chuan感gan器qi並bing非fei損sun耗hao型xing的de,因yin此ci無wu需xu對dui傳chuan感gan器qi進jin行xing特te別bie保bao護hu,在zai非fei試shi驗yan時shi間jian保bao持chi測ce試shi腔qiang內nei幹gan燥zao潔jie淨jing即ji可ke。若ruo在zai很hen長chang一yi段duan時shi間jian內nei不bu用yong儀yi器qi時shi,需xu要yao將jiang測ce試shi濕shi腔qiang中zhong的de加jia濕shi物wu質zhi取qu出chu,並bing用yong幹gan燥zao濾lv紙zhi把ba附fu著zhe在zai腔qiang壁bi上shang的de水shui吸xi幹gan。同tong樣yang濕shi度du傳chuan感gan器qi法fa也ye應ying注zhu意yi對dui試shi驗yan尾wei氣qi的de處chu理li,而er且qie加jia濕shi物wu質zhi應ying使shi用yong指zhi定ding的de蒸zheng餾liu水shui或huo者zhe試shi劑ji。
3. 總結
縱上所述,壓差法、稱重法、以及濕度傳感器法維護方便簡單,隻需進行常規的維護操作就可以了。但是對於等壓法、紅外傳感器法、以及電解傳感器法必須注意傳感器的保護、試驗尾氣的處理、測(ce)試(shi)係(xi)統(tong)內(nei)雜(za)質(zhi)氣(qi)體(ti)的(de)清(qing)除(chu)等(deng)幾(ji)個(ge)方(fang)麵(mian),操(cao)作(zuo)必(bi)須(xu)嚴(yan)謹(jin)仔(zai)細(xi),否(fou)則(ze)將(jiang)會(hui)引(yin)起(qi)傳(chuan)感(gan)器(qi)壽(shou)命(ming)的(de)衰(shuai)減(jian),考(kao)慮(lv)到(dao)傳(chuan)感(gan)器(qi)使(shi)用(yong)成(cheng)本(ben)不(bu)菲(fei),因(yin)此(ci)對(dui)這(zhe)些(xie)測(ce)試(shi)設(she)備(bei)進(jin)行(xing)特(te)別(bie)維(wei)護(hu)就(jiu)更(geng)加(jia)有(you)必(bi)要(yao)了(le)。
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