(1)電子天平
電dian子zi天tian平ping是shi我wo們men的de化hua學xue實shi驗yan中zhong必bi備bei的de稱cheng量liang工gong具ju,學xue生sheng也ye基ji本ben能neng掌zhang握wo其qi使shi用yong方fang法fa,但dan實shi驗yan的de細xi節jie和he打da掃sao維wei護hu做zuo的de很hen不bu到dao位wei,實shi驗yan後hou秤cheng盤pan下xia殘can留liu有you一yi些xie物wu質zhi,秤cheng盤pan上shang留liu有you汙wu漬zi。使shi天tian平ping的de靈ling敏min度du和he準zhun確que度du下xia降jiang,使shi用yong壽shou命ming也ye縮suo短duan。電dian子zi天tian平ping使shi用yong前qian須xu先xian預yu熱re10fenzhong,danbufenxueshengkaijihouzhijiechengliang。chengliangwudewendubixuyutianpingwenduxiangtong,bunengbaguorehuoguolengdewutifangzaitianpingchengpanshang。yixiejuyouhuifaxingdefushixingdeshijiyingfangzaimibirongqizhongchengliang,chengliangwutishiyaoqiejiguanbitianpingdecemen,chengliangwanbihoujishidasaochengliangpanshangxiajigegejiaoluodeng。zaikongqichaoshi,wuzhiyijiechenggoukuaishi,yingcaiyongjixiechuxiufangfa,jixianyongchan、剔、刮等方式將零部件上的鏽蝕層塊除去,再用砂紙砂磨、打光,最後塗上保護層。實驗完畢,關閉側門,蓋上天平布,置於避光幹燥處保存。
(2)電熱恒溫幹燥箱
電熱恒溫幹燥箱是化學實驗中用於對物品進行烘焙、幹燥的常規儀器。幹燥箱的工作電壓為220V,溫度為100-110度du,不bu宜yi過guo高gao。可ke燃ran性xing和he揮hui發fa性xing的de化hua學xue物wu品pin切qie勿wu放fang入ru箱xiang內nei,箱xiang內nei載zai物wu應ying擺bai放fang應ying在zai隔ge板ban的de較jiao中zhong心xin部bu位wei,同tong時shi不bu影ying響xiang空kong氣qi流liu通tong以yi保bao證zheng箱xiang內nei溫wen度du均jun勻yun。幹gan燥zao箱xiang使shi用yong過guo程cheng中zhong,學xue生sheng不bu能neng用yong濕shi手shou觸chu摸mo箱xiang體ti和he開kai關guan。幹gan燥zao箱xiang正zheng常chang運yun行xing時shi如ru在zai使shi用yong過guo程cheng中zhong出chu現xian異yi常chang、氣味、煙yan霧wu等deng情qing況kuang,應ying立li即ji關guan閉bi電dian源yuan,請qing專zhuan業ye人ren員yuan查zha看kan修xiu理li。箱xiang壁bi內nei膽dan和he設she備bei表biao麵mian要yao經jing常chang擦ca拭shi,以yi保bao持chi清qing潔jie,增zeng加jia玻bo璃li的de透tou明ming度du。幹gan燥zao箱xiang若ruo長chang期qi不bu用yong,應ying拔ba掉diao電dian源yuan線xian以yi防fang止zhi設she備bei損sun傷shang人ren,並bing應ying定ding期qi按an使shi用yong條tiao件jian運yun行xing2-3天,以驅除電器部分的潮氣,避免損壞有關器件。
(3)恒溫水浴鍋
恒溫水浴鍋主要用於實驗室中蒸餾,幹燥,濃縮化學藥品,也可用於恒溫加熱和其它溫度試驗,是化學實驗室、分析室、教(jiao)育(yu)科(ke)研(yan)的(de)必(bi)備(bei)工(gong)具(ju)。在(zai)使(shi)用(yong)中(zhong)學(xue)生(sheng)應(ying)該(gai)知(zhi)道(dao)它(ta)的(de)使(shi)用(yong)方(fang)法(fa)及(ji)注(zhu)意(yi)事(shi)項(xiang),以(yi)便(bian)實(shi)驗(yan)能(neng)夠(gou)順(shun)利(li)進(jin)行(xing)。加(jia)水(shui)之(zhi)前(qian)切(qie)勿(wu)接(jie)通(tong)電(dian)源(yuan),最(zui)好(hao)加(jia)入(ru)蒸(zheng)餾(liu)水(shui),以(yi)免(mian)產(chan)生(sheng)水(shui)垢(gou),加(jia)水(shui)不(bu)要(yao)太(tai)多(duo),以(yi)免(mian)沸(fei)騰(teng)時(shi)水(shui)量(liang)溢(yi)出(chu)鍋(guo)外(wai);鍋內水量也不可低於二分之一,不能使加熱管露出水麵;qiewuwushuihuoshuiweidiyugebanjiare,fouzehuisunhuaijiareguan。zhushuishibunengjiangshuiliurukongzhixiangnei,yifangfashengchudian。ruhengwenkongzhishiling,kejiangkongzhiqishangdeyinjiedianyongxishabucaliang。shiyongwanbihou,quchuhengwenwu,guanbidianyuan,paichuxiangtineideshui,zuohaoyiqishiyongjilu。
(1)燒杯
燒杯因其口徑上下一致,是取用液體、配製溶液、zuojiandanhuaxuefanyingzuichangyongdefanyingrongqi。danshaobeibunengdaitiliangtongliangquyeti。shaobeijiareshiyaodianshangshimianwang。bunengyonghuoyanzhijiejiareshaobei。yinweishaobeidimianda,yonghuoyanzhijiejiare,zhikeshaodaojubu,shibolishourebuyuneryinqizhalie。yongshaobeijiareyetishi,yetideliangyibuchaoguoshaobeirongjide1/3weiyi,yifangfeitengshiyetiwaiyi。jiareshi,shaobeiwaibixucagan。jiarefushixingyaopinshi,kejiangyibiaomianmingaizaishaobeikoushang,yimianyetijianchu。bukeyongshaobeichangqishengfanghuaxueyaopin,yimianluoruchentuheshirongyezhongdeshuifenzhengfa。rongjiehuoxishiguochengzhong,yongbolibangjiaobanshi,buyaochujibeidihuobeibi。
(2)試管
實驗室用來盛放少量藥品,加熱情況下少量試劑反應的容器。裝溶液時不超過試管容量的1/2,加熱時不超過試管的1/3。取塊狀固體放入試管要用鑷子,不能使固體直接墜入試管中,防止試管底破裂。加熱時使用試管夾,試管夾應夾在距管口1/3處。試管口不能對著人。試管不可以直接加熱,要先預熱,加熱盛有固體的試管時,管口略向下,加熱液體時傾斜約45°。jiareshiyaobaochishiguanwaibimeiyoushuizhu,fangzhishourebujunyunerbaolie。jiarehoubunengzhouleng,fangzhishiguanpolie。jiarehoubunengzaishiguanweilengquezhishiwenshijiuxidishiguan。jiareshiyingyongwaiyan。
(3)容量瓶
容(rong)量(liang)瓶(ping)主(zhu)要(yao)用(yong)於(yu)準(zhun)確(que)地(di)配(pei)製(zhi)一(yi)定(ding)摩(mo)爾(er)濃(nong)度(du)的(de)溶(rong)液(ye),它(ta)是(shi)一(yi)種(zhong)細(xi)長(chang)頸(jing),梨(li)形(xing)的(de)平(ping)底(di)玻(bo)璃(li)瓶(ping),帶(dai)有(you)磨(mo)口(kou)玻(bo)璃(li)塞(sai),瓶(ping)頸(jing)上(shang)刻(ke)有(you)標(biao)線(xian),當(dang)瓶(ping)內(nei)液(ye)體(ti)在(zai)所(suo)指(zhi)定(ding)溫(wen)度(du)下(xia)達(da)到(dao)標(biao)線(xian)處(chu)時(shi),其(qi)體(ti)積(ji)即(ji)為(wei)瓶(ping)上(shang)所(suo)注(zhu)明(ming)的(de)容(rong)積(ji)數(shu)。容(rong)量(liang)瓶(ping)不(bu)能(neng)配(pei)製(zhi)其(qi)容(rong)積(ji)以(yi)下(xia)體(ti)積(ji)的(de)溶(rong)液(ye),即(ji)其(qi)容(rong)積(ji)為(wei)多(duo)大(da),就(jiu)隻(zhi)能(neng)配(pei)製(zhi)多(duo)大(da)體(ti)積(ji)的(de)溶(rong)液(ye)。容(rong)量(liang)瓶(ping)使(shi)用(yong)前(qian)應(ying)先(xian)檢(jian)查(zha)是(shi)否(fou)漏(lou)水(shui),依(yi)次(ci)用(yong)自(zi)來(lai)水(shui),蒸(zheng)餾(liu)水(shui)洗(xi)好(hao)備(bei)用(yong)。將(jiang)溶(rong)質(zhi)在(zai)燒(shao)杯(bei)中(zhong)溶(rong)解(jie)後(hou)轉(zhuan)移(yi)到(dao)容(rong)量(liang)瓶(ping)裏(li),不(bu)能(neng)在(zai)容(rong)量(liang)瓶(ping)裏(li)進(jin)行(xing)溶(rong)質(zhi)的(de)溶(rong)解(jie),控(kong)製(zhi)溶(rong)解(jie)溶(rong)質(zhi)的(de)蒸(zheng)餾(liu)水(shui)量(liang)。轉(zhuan)移(yi)時(shi)必(bi)須(xu)用(yong)玻(bo)璃(li)棒(bang)引(yin)流(liu)。容(rong)量(liang)瓶(ping)不(bu)能(neng)進(jin)行(xing)加(jia)熱(re),如(ru)果(guo)溶(rong)質(zhi)在(zai)溶(rong)解(jie)過(guo)程(cheng)中(zhong)放(fang)熱(re),要(yao)待(dai)溶(rong)液(ye)冷(leng)卻(que)後(hou)再(zai)進(jin)行(xing)轉(zhuan)移(yi),因(yin)為(wei)溫(wen)度(du)升(sheng)高(gao)瓶(ping)體(ti)將(jiang)膨(peng)脹(zhang),所(suo)量(liang)體(ti)積(ji)就(jiu)會(hui)不(bu)準(zhun)確(que)。用(yong)於(yu)洗(xi)滌(di)燒(shao)杯(bei)的(de)溶(rong)劑(ji)總(zong)量(liang)不(bu)能(neng)超(chao)過(guo)容(rong)量(liang)瓶(ping)的(de)標(biao)線(xian),一(yi)旦(dan)超(chao)過(guo),必(bi)須(xu)重(zhong)新(xin)進(jin)行(xing)配(pei)置(zhi)。配(pei)製(zhi)好(hao)的(de)溶(rong)液(ye)轉(zhuan)移(yi)至(zhi)試(shi)劑(ji)瓶(ping)中(zhong)保(bao)存(cun),容(rong)量(liang)瓶(ping)隻(zhi)能(neng)配(pei)製(zhi)溶(rong)液(ye),不(bu)能(neng)儲(chu)存(cun)溶(rong)液(ye),因(yin)為(wei)溶(rong)液(ye)可(ke)能(neng)會(hui)對(dui)瓶(ping)體(ti)進(jin)行(xing)腐(fu)蝕(shi),從(cong)而(er)使(shi)容(rong)量(liang)瓶(ping)的(de)精(jing)度(du)受(shou)到(dao)影(ying)響(xiang)。容(rong)量(liang)瓶(ping)使(shi)用(yong)完(wan)畢(bi)應(ying)及(ji)時(shi)用(yong)水(shui)衝(chong)洗(xi)幹(gan)淨(jing),塞(sai)上(shang)瓶(ping)塞(sai),並(bing)在(zai)塞(sai)子(zi)與(yu)瓶(ping)口(kou)之(zhi)間(jian)夾(jia)一(yi)條(tiao)紙(zhi)條(tiao),防(fang)止(zhi)瓶(ping)塞(sai)與(yu)瓶(ping)口(kou)粘(zhan)連(lian)。最(zui)後(hou)記(ji)錄(lu)溶(rong)液(ye)體(ti)積(ji)的(de)時(shi)候(hou)一(yi)般(ban)保(bao)留(liu)4位有效數字(XXX.0mL)。
(4)滴定管
滴定管是可放出不固定量液體的量出式玻璃儀器,主要用於滴定分析中對滴定劑體積的測量。能精確到0.01mL。帶玻璃活塞的滴定管為酸式滴定管,帶有內裝玻璃球的橡皮管的滴定管為堿式滴定管。酸式、堿式滴定管不能混用,酸式滴定管裝酸性物質和大多數中性物質(尤其是強氧化劑),堿式滴定管裝堿性物質(包括堿和堿性鹽),滴定管使用前先檢查是否漏液,如果漏水,應重新將活塞塗凡士林油。裝液前要用洗液、水(shui)依(yi)次(ci)衝(chong)洗(xi)幹(gan)淨(jing),並(bing)要(yao)用(yong)待(dai)裝(zhuang)的(de)溶(rong)液(ye)潤(run)洗(xi)滴(di)定(ding)管(guan)。將(jiang)操(cao)作(zuo)溶(rong)液(ye)倒(dao)入(ru),直(zhi)到(dao)充(chong)滿(man)至(zhi)零(ling)刻(ke)度(du)線(xian)以(yi)上(shang)為(wei)止(zhi)。注(zhu)意(yi)檢(jian)查(zha)滴(di)定(ding)管(guan)的(de)出(chu)口(kou)管(guan)是(shi)否(fou)充(chong)滿(man)溶(rong)液(ye),如(ru)有(you)氣(qi)泡(pao)進(jin)行(xing)排(pai)氣(qi)泡(pao)操(cao)作(zuo)。調(tiao)整(zheng)液(ye)麵(mian)時(shi),使(shi)液(ye)麵(mian)保(bao)持(chi)在(zai)“0”或“0”以(yi)下(xia)的(de)某(mou)一(yi)定(ding)刻(ke)度(du)。進(jin)行(xing)滴(di)定(ding)時(shi),應(ying)將(jiang)滴(di)定(ding)管(guan)垂(chui)直(zhi)地(di)夾(jia)在(zai)滴(di)定(ding)管(guan)夾(jia)上(shang),如(ru)使(shi)用(yong)的(de)是(shi)堿(jian)式(shi)滴(di)定(ding)管(guan),拇(mu)指(zhi)與(yu)食(shi)指(zhi)在(zai)玻(bo)璃(li)珠(zhu)所(suo)在(zai)部(bu)位(wei)一(yi)旁(pang)捏(nie)乳(ru)膠(jiao)管(guan),不(bu)要(yao)捏(nie)玻(bo)璃(li)珠(zhu),也(ye)不(bu)能(neng)使(shi)其(qi)上(shang)下(xia)移(yi)動(dong)。滴(di)定(ding)時(shi)應(ying)逐(zhu)滴(di)連(lian)續(xu)滴(di)加(jia),接(jie)近(jin)終(zhong)點(dian)時(shi),隻(zhi)加(jia)一(yi)滴(di)或(huo)半(ban)滴(di),至(zhi)溶(rong)液(ye)出(chu)現(xian)明(ming)顯(xian)的(de)顏(yan)色(se)變(bian)化(hua)。讀(du)數(shu)時(shi),手(shou)拿(na)滴(di)定(ding)管(guan)上(shang)部(bu)無(wu)刻(ke)度(du)處(chu),使(shi)滴(di)定(ding)管(guan)保(bao)持(chi)垂(chui)直(zhi),視(shi)線(xian)平(ping)視(shi)溶(rong)液(ye)的(de)凹(ao)液(ye)麵(mian),讀(du)到(dao)小(xiao)數(shu)點(dian)後(hou)第(di)二(er)位(wei),即(ji)估(gu)計(ji)到(dao)0.01mL。滴定結束後,管內剩餘的溶液應棄去,不得將其倒回原瓶,隨即清洗滴定管,並倒掛於鐵架台上。
實驗室常用的玻璃儀器如燒杯、試管、滴定管、移液管、容量瓶等。儀器在使用中會沾上油汙,水垢,鏽跡等,使用後不及時完全的清洗,會造成結果誤差,甚至會對儀器的壽命、性能會產生極其不良的影響。因此,化學實驗使用的玻璃儀器必須洗滌幹淨。下麵介紹一些玻璃儀器的洗滌方法。
附fu有you易yi去qu除chu物wu質zhi的de簡jian單dan儀yi器qi,如ru試shi管guan。燒shao杯bei等deng,先xian用yong自zi來lai水shui衝chong洗xi,再zai用yong試shi管guan刷shua蘸zhan取qu合he成cheng洗xi滌di劑ji刷shua洗xi,最zui後hou自zi來lai水shui衝chong洗xi。當dang倒dao置zhi儀yi器qi,器qi壁bi形xing成cheng一yi層ceng均jun勻yun的de水shui膜mo,不bu成cheng股gu流liu下xia時shi,即ji已yi洗xi淨jing。
有油汙的玻璃器皿,先用堿性酒精洗滌液洗滌,然後用洗衣粉水或肥皂水洗滌,再用自來水衝洗幹淨。
有鏽跡,水垢的器皿,用(1+3)鹽酸洗液浸泡,再用再來水衝洗幹淨。
有凡士林油汙的器皿,先將凡士林擦去,再用洗衣粉水或肥皂水洗燒煮,取出後用自來水衝洗幹淨。
一些構造比較精細、複雜的玻璃儀器,如容量瓶、移液管等,無法用毛刷刷洗,可以用洗滌液浸泡一定時間,再進行清洗。
洗淨的玻璃儀器不要再用手、布或紙擦拭,以免重新汙染。
實驗室常用的光學儀器如分光光度計、折光計的棱鏡、玻片等,都是一些精密光學儀器,在使用和保養中,必須細心謹慎,嚴格按說明使用,不得任意鬆動儀器各連接部分,不得跌落、碰peng撞zhuang儀yi器qi,以yi防fang止zhi光guang學xue零ling件jian損sun傷shang及ji影ying響xiang精jing度du。被bei測ce試shi樣yang中zhong不bu應ying有you硬ying性xing雜za質zhi,當dang測ce試shi固gu體ti試shi樣yang時shi,應ying防fang止zhi把ba折zhe射she棱leng鏡jing表biao麵mian拉la毛mao或huo產chan生sheng壓ya痕hen。使shi用yong完wan畢bi後hou,嚴yan禁jin直zhi接jie放fang入ru水shui中zhong清qing洗xi,避bi免mian光guang學xue係xi統tong管guan路lu進jin水shui。打da開kai棱leng鏡jing,用yong擦ca鏡jing紙zhi輕qing輕qing擦ca幹gan,不bu論lun在zai任ren何he情qing況kuang下xia,不bu允yun許xu用yong擦ca鏡jing紙zhi以yi外wai的de任ren何he東dong西xi接jie觸chu到dao棱leng鏡jing,以yi免mian損sun壞huai它ta的de光guang學xue平ping麵mian。儀yi器qi應ying存cun放fang於yu幹gan燥zao、無灰塵、無油汙和無有害、易燃、易爆等氣體的地方,以免光學零件腐蝕或生黴。
光學儀器在使用中容易沾上油汙、水濕性汙物、指紋等,影響成像及透光率。清洗折光計的棱鏡、平麵鏡、xianweijingdejingtou,xianyongzhengliushuijinxingqingxi,jingmianruoyouwuzi,keyiyongyichunheyimidehunheyeqingxi。qingxishiyongzhuanmendecajingzhihuomianqiuzhanyoushaoliangqingxiji,shunzheyigefangxiangcashi,congjingtouzhongxinxiangwaizuoyuanyundong,qiejibazheleijingtoujinpaozaiqingxijizhongqingxi。qingxijingtoubudeyonglishica,fouzehuihuashangzengtoumo,sunhuaijingtou。qingxiwanbihouyongcajingzhicagan,biguangbaocun。
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